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Crystal data for 1: Orthorhombic, space group Pmn2 1, a, 16.177(2) Å, b, 12.7249(17) Å, c, 13.1859(18) Å, V, 2714.2(6, Å3, Z, 2, Dc, 4.104 mg/m3, μ, 26.242 mm-1, F(000, 2918, T, 194.5(2) K, R1 0.0315, wR 2, 0.0826, GOF, 1.093 for 14824 reflections measured, 4682 unique [Rint, 0.0407, 364 parameters with I > 2σ(I) in the range of 1.60 < θ < 26.05°
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int = 0.0407], 364 parameters with I > 2σ(I) in the range of 1.60 < θ < 26.05°.
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Oa refers to central oxygen atom; Ob refers to bridging oxygen atom; Ot refers to terminal oxygen atoms; Ot′ are terminal oxygen atoms linked to Ln3
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3+.
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