A synthetic equivalent of a germanone derivative

European Journal of Inorganic Chemistry

Volumn , Issue 27, 2008, Pages 4242-4247

  Bonnefille, Eric ^a   Mazières, Stéphane ^a   Bibal, Christine ^a   Saffon, Nathalie ^a   Gornitzka, Heinz ^a   Couret, Claude ^a  

^a UNIVERSITÉ PAUL SABATIER   (France)

Author keywords

Alcohols; Fluorine; Germanium; Germanolate; Germanone

Indexed keywords

ATOMS; CHELATION; CRYSTAL STRUCTURE; FLUORINE; FLUORINE COMPOUNDS; GERMANIUM; GERMANIUM COMPOUNDS; HYDROGEN; KETONES; LITHIUM COMPOUNDS; SINGLE CRYSTALS;

COLORLESS CRYSTALS; GERMANES; GERMANIUMS (GE); GERMANOLATE; GERMANONE; LOWS-TEMPERATURES; MOLAR EQUIVALENT; PHENYLLITHIUM; SINGLE-CRYSTAL STRUCTURE ANALYSIS; SYNTHETIC EQUIVALENTS;

TEMPERATURE;

EID: 53449102963     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.200800494     Document Type: Article

References (40)

1. M. Massol, D. Mesnard, J. Barrau, J. Satgé, C. R. Acad. Sci., Ser. C 1971, 272, 2081-2084.
2. For selected reviews on heavy ketones, see: a) J. Barrau, G. Rima, Coord. Chem. Rev. 1998, 178-180, 593-622;
3. b) R. Okazaki, N. Tokitoh, Acc. Chem. Res. 2000, 33, 625-630;
4. c) N. Tokitoh, R. Okazaki, Adv. Organometallic. Chem. 2001, 47, 121-166;
5. d) N. Takeda, N. Tokitoh, R. Okazaki, Handbook of Chalcogen Chemistry (Ed.: F. A. Devillanova), The Royal Society of Chemistry, Cambridge, 2007, chapter 3, pp. 195-222.
6. J. Barrau, M. Bouchaut, A. Castel, A. Cazes, G. Dousse, H. Lavayssière, P. Rivière, J. Satgé, Synth. React. Inorg. Met-Org. Chem. 1979, 9, 273-288.
7. J. Barrau, M. Bouchaut, H. Lavayssière, G. Dousse, J. Satgé, Helv. Chim. Acta 1979, 62, 152-154.
8. P. Rivière, J. Satgé, A. Castel, A. Cazes, J. Organomet. Chem. 1979, 177, 171-180.
9. R. Withnall, L. Andrews, J. Phys. Chem. 1990, 94, 2351-2357.
10. V. N. Khabashesku, S. E. Boganov, K. N. Kudin, J. L. Margrave, O. M. Nefedov, Organometallics 1998, 17, 5041-5051.
11. a) T. Matsumoto, N. Tokitoh, R. Okazaki, Chem. Commun. 1997, 1553-1554;
12. b) N. Tokitoh, T. Matsumoto, R. Okazaki, Bull. Chem. Soc. Jpn. 1999, 72, 1665-1684.
13. K. Kishikawa, N. Tokitoh, R. Okazaki, Chem. Lett. 1996, 695-696.
14. a) D. Ellis, P. B. Hitchcock, M. F. Lappert, J. Chem. Soc., Dalton Trans. 1992, 3397-3398;
15. b) N. Tokitoh, K. Kishikawa, R. Okazaki, T. Sasamori, N. Nakata, N. Takeda, Polyhedron 2002, 21, 563-577;
16. c) P. Jutzi, H. Schmidt, B. Neumann, H.-G. Stammler, Organometallics 1996, 15, 741-746;
17. d) M. Veith, A. Rammo, Z. Anorg. Allg. Chem. 1997, 623, 861-872.
18. J. Barrau, M. Massol, D. Mesnard, J. Satgé, J. Recueil Trav. Chim. Pays-Bas 1973, 92, 321-339.
19. H. Lavayssière, J. Barrau, G. Dousse, J. Satgé, M. Bouchaut, J. Organomet. Chem. 1978, 154, C9-C12.
20. L. Pu, N. J. Hardman, P. P. Power, Organometallics 2001, 20, 5105-5109.
21. N. Tokitoh, T. Matsumoto, R. Okazaki, Chem. Lett. 1995, 1087-1088.
22. G. L. Wegner, R. T. F. Berger, A. Schier, H. Schmidbaur, Organometallics 2001, 20, 418-423.
23. C. Bibal, S. Mazières, H. Gornitzka, C. Couret, Polyhedron 2002, 21, 2827-2834.
24. C. Bibal, S. Mazières, H. Gornitzka, C. Couret, Angew. Chem. Int. Ed. 2001, 40, 952-954.
25. W. C. Hamilton, J. A. Ibers, Hydrogen Bonding in Solids: Methods of Molecular Structure Determination, W. A. Benjamin, New York, 1968, p. 16.
26. a) K. M. Baines, W. G. Stibbs, Coord. Chem. Rev. 1995, 145, 157-200.
27. For recent examples of Ge-F bond lengths, see: b) K. Iwanaga, J. Kobayashi, T. Kawashima, N. Takagi, S. Nagase, Organometallics 2006, 25, 3388-3393 (1.744, 1.748 and 1.839 Å);
28. c) P. D. Prince, G. S. McGrady, J. W. Steed, New J. Chem. 2002, 26, 457-461 (1.749 Å).
29. H. Puff, S. Franken, W. Schuh, W. Schwab, J. Organomet. Chem. 1983, 254, 33-41.
30. J. Beckmann, K. Jurkschat, M. Schürmann, Eur. J. Inorg. Chem. 2000, 939-941.
31. C. Glidewell, M. B. Hursthouse, D. Lloyd, K. W. Lumbard, R. L. Short, J. Chem. Res. (S) 1986, 11, 400-401.
32. H.-C. Chiang, S.-M. Lin, C.-H. Ueng, Acta Crystallogr., Sect. C 1992, 48, 991-993.
33. S.-J. Lin, Y.-J. Chen, J.-H. Chen, F.-L. Liao, S.-L. Wang, S.-S. Wang, Polyhedron 1997, 16, 2843-2850.
34. G. Duverneuil, P. Mazerolles, E. Perrier, Appl. Organomet. Chem. 1994, 8, 119-127.
35. S. Masamune, Y. Hanzawa, J. Am. Chem. Soc. 1982, 104, 6136-6137.
36. L. Fajari, J. Carilla, L. Julia, J. Riera, A. Parraga, M. Coll, J. Organomet. Chem. 1994, 474, 89-95.
37. J. M. Miller, J. H. Clark, J. Chem. Soc., Chem. Commun. 1982, 1318-1319.
38. O. H. Johnson, H. E. Fritz, J. Am. Chem. Soc. 1953, 75, 718-720.
39. a) SHELXS-97: G. M. Sheldrick, Acta Crystallogr., Sect. A 1990, 46, 467-473;
40. b) G. M. Sheldrick, SHELXL-97: Program for Crystal Structure Refinement, University of Göttingen, 1997.