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51
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85163230258
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SIR97: A. Altomare, M. C. Burla, G. M. Camalli, G. Cascarano, C. Giacovazzo, A. Guagliardi, A. G. G. Moliterni, G. Polidori, R. Spagna, J. Appl. Crystallogr. 1999, 32, 115.
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52
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0004150157
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SHELXL-97
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55
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85163234283
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-
Crystal data for 1(MeOH)0.25: C113H 108Fe4N16O17, Mr, 2185.56 gmol-1, size 0.26x0.12x0.06 mm, triclinic, space group P1, a, 11.5638(2, b, 19.6799(6, c, 23.3958(7) Å, α, 79.759(1, β, 87.859(2, γ, 79.830(2)°, V, 5157.0(2) Å3, Z, 2, ρcalcd, 1.404 gcm-3, μ (Mo-Kα, 0.71073 Å, F(000, 2266, 44624 reflections in h, 15/13, k, 25/25, l, 30/30, measured in the range 3.17° ≤ θ ≤ 27.57°, 23592 independent reflections, 10861 reflections with F o> 4σFo, 639 parameters, 0 restraints R1all, 0.2995, wR2all, 0.5320
-
2all = 0.5320.
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-
-
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