ZnCl3(4-methyl-4,4′-bipyridinium) with 4-methyl-4,4′-bipyridinium generated in situ: synthesis, structure and photoluminescence

Inorganic Chemistry Communications

Volumn 11, Issue 10, 2008, Pages 1212-1214

  Chen, Wen Tong ^a   Liu, Dong Sheng ^a   Ying, Shao Ming ^a   Chen, Hua Long ^a   Xu, Ya Ping ^a  

^a JINGGANGSHAN UNIVERSITY   (China)

Author keywords

Bipyridine; In situ; Photoluminescence; Viologen; Zinc

Indexed keywords

EID: 53149100813     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2008.07.011     Document Type: Article

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13. 2 (1 mmol, 0.136 g), 4,4′-bipyridine (1 mmol, 0.156 g), concentrated HCl acid (1 mL), methanol (2 mL) and distilled water (7 mL) in a 25 mL Teflon-lined stainless steel autoclave and heated at 200 °C for 7 days. After being slowly cooled to room temperature at 6 °C/h, colorless crystals suitable for X-ray analysis were obtained. The yield was 86% (based on zinc).
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