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Crystal structure data for 1·2H2O·4. 5MeCN: C81H71.5Cu6N18.5O 18, Mw, 1973.31, triclinic, space group P1 with a, 16.289(8) Å, b, 17.295(8) Å, c, 18.125(8) Å, α, 69.870(10)°, β, 69.18(2)°, γ, 73.48(2)°, V, 4404(4) Å3, T, 298 K, Z, 2, R1 [I > 2σ(I, 0.0711, wR2, 0.1396 (F2, all data, Crystal structure data for 2: C38H32Cu 4N16O8, Mw, 1094.96, monoclinic, space group P21/c with a, 21.690(10) Å, b, 12.867(9) Å, c, 16.810(10) Å, β, 114.46(2)°, V, 4270(4) Å3, T, 298 K, Z, 4, R1 [I > 2
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2, all data).
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