High-resolution 14N-edited 1H-13C correlation NMR experiment to study biological solids

Journal of Magnetic Resonance

Volumn 194, Issue 2, 2008, Pages 317-320

  Amoureux, Jean Paul ^a   Trébosc, Julien ^a   Hu, Bingwen ^a   Halpern Manners, Nicholas ^b   Antonijevic, Sasa ^c,d  

^a UNITÉ DE CATALYSE ET DE CHIMIE DU SOLIDE   (France)

^b UNIVERSITY OF CALIFORNIA   (United States)

^c University of California   (United States)

^d LAWRENCE BERKELEY NATIONAL LABORATORY   (United States)

Author keywords

2D correlation; Amino acids; Coherence transfer; Nitrogen 14; Solid state NMR

Indexed keywords

MAGNETIC RESONANCE; NITROGEN; NONMETALS; NUCLEAR MAGNETIC RESONANCE; RESONANCE; SPIN DYNAMICS;

2D CORRELATION; AMINO ACIDS; COHERENCE TRANSFER; DECOUPLING TECHNIQUES; DIPOLAR DECOUPLING; DIPOLAR RECOUPLING; HIGH RESOLUTIONS; INDIRECT DETECTION; MAGIC ANGLE; RECOUPLING; SOLID-STATE NMR;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

BIOPOLYMER; CARBON; HISTIDINE; NITROGEN; PROTON;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY;

BIOPOLYMERS; CARBON ISOTOPES; HISTIDINE; MAGNETIC RESONANCE SPECTROSCOPY; NITROGEN; PROTONS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 52949092445     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2008.07.021     Document Type: Article

References (26)

1. 14N MAS NMR spectroscopy and quadrupole coupling data in characterization of the IV-III phase transition in ammonium nitrate. J. Phys. Chem. B 106 (2002) 3026-3032
2. 14N magic-angle spinning NMR study of some amino acids. J. Magn. Reson. 166 (2004) 262-272
3. 14N solid-state NMR spectroscopy. Angew. Chem. Int. Ed. 37 (1998) 1282-1283
4. 14N nuclear magnetic resonance of polycrystalline solids with fast spinning at or very near the magic angle. J. Chem. Phys. 111 (1999) 8963-8969
5. 14N MAS NMR of ammonium ions as a spy to structural insights for ammonium salts. Magn. Reson. Chem. 44 (2006) 348-356
6. Tycko R., and Opella S.J. High-resolution nitrogen-14 overtone spectroscopy: an approach to natural abundance nitrogen NMR of oriented and polycrystalline systems. J. Am. Chem. Soc. 108 (1986) 3531-3532
7. Tycko R., and Opella S.J. Overtone NMR spectroscopy. J. Chem. Phys. 86 (1987) 1761-1774
8. Tycko R., Stewart P.L., and Opella S.J. Peptide plane orientations determined by fundamental and overtone nitrogen-14 NMR. J. Am. Chem. Soc. 108 (1986) 5419-5425
9. 13C NMR correlation under magic-angle spinning. J. Am. Chem. Soc. 128 (2006) 6040-6041
10. Cavadini S., Lupulescu A., Antonijevic S., and Bodenhausen G. Nitrogen-14 NMR spectroscopy using residual dipolar splittings in solids. J. Am. Chem. Soc. 128 (2006) 7706-7707
11. Cavadini S., Antonijevic S., Lupulescu A., and Bodenhausen G. Indirect detection of nitrogen-14 in solids via protons by nuclear magnetic resonance spectroscopy. J. Magn. Reson. 182 (2006) 168-172
12. 14N heteronuclear multiple-quantum correlation with rotary resonance and REDOR dipolar recoupling. J. Magn. Reson. 184 (2006) 39-43
13. 14N MAS NMR using homonuclear decoupled rotary resonance. Chem. Phys. Lett. 435 (2007) 163-169
14. 14N correlation solid-state NMR spectrum. J. Magn. Reson. 193 (2008) 321-325
15. Schmidt-Rohr K., and Mao J.D. Selective observation of nitrogen-bonded carbons in solid-state NMR by saturation-pulse induced dipolar exchange with recoupling. Chem. Phys. Lett. 359 (2002) 403-411
16. Fu R., Smith S.A., and Bodenhausen G. Recoupling of heteronuclear dipolar interactions in solid-state MAS NMR by simultaneous frequency and amplitude modulation. Chem. Phys. Lett. 272 (1997) 361-369
17. Hu B., Trebosc J., and Amoureux J.P. Comparison of several hetero-nuclear recoupling NMR methods to be used in MAS HMQC/HSQC. J. Magn. Reson. 192 (2008) 112
18. Amoureux J.P., Hu B., and Trebosc J. Enhanced resolution in proton solid-state NMR with very-fast MAS experiments. J. Magn. Reson. 193 (2008) 305-307
19. Levitt M.H., Oas T.G., and Griffin R.G. Rotary resonance recoupling in heteronuclear spin pair systems. Isr. J. Chem. 28 (1988) 271-282
20. Oas T.G., Griffin R.G., and Levitt M.H. Rotary resonance recoupling of dipolar interactions in solid-state nuclear magnetic resonance spectroscopy. J. Chem. Phys. 89 (1988) 692-695
21. Nielsen N.C., Bildsoe H., Jakobsen H.J., and Levitt M.H. Double-quantum homonuclear rotary resonance: efficient dipolar recovery in magic-angle spinning nuclear magnetic resonance. J. Chem. Phys. 101 (1994) 1805-1812
22. Carravetta M., Eden M., Zhao X., Brinkmann A., and Levitt M.H. Symmetry principles for the design of radiofrequency pulse sequences in the nuclear magnetic resonance of rotating solids. Chem. Phys. Lett. 321 (2000) 205-215
23. O. Lafon, B. Hu, Q. Wang, J. Trebosc, J.P. Amoureux, in preparation.
24. Fung B.M., Khintrin A.K., and Ermolaev K. An improved decoupling sequence for liquid crystals and solids. J. Magn. Reson. 142 (2000) 97-101
25. Madhu P.K., Vinogradov E., and Vega S. Multiple-pulse and magic-angle spinning aided double-quantum proton solid-state NMR spectroscopy. Chem. Phys. Lett. 394 (2004) 423-428
26. Kervern G., Pintacuda G., and Emsley L. Fast adiabatic pulses for solid-state NMR of paramagnetic systems. Chem. Phys. Lett. 435 (2007) 157-162