Metallaheteroborane chemistry. Part 5. Synthesis of closo-[2,2-(PR3)2-1,2-SePtB10H 10](R3 = Et3, Bun3 or Me2Ph) and arachno-[9,9-(PMe2Ph)2-6,9-SePtB8H 10] and their characterisation by nuclear magnetic resonance techniques

Journal of the Chemical Society, Dalton Transactions

Volumn , Issue 9, 1989, Pages 1657-1668

  Faridoon, ^a   Ni Dhubhghaill, Orla ^a   Spalding, Trevor R ^a   Ferguson, George ^b   Kaitner, Branko ^b   Fontaine, Xavier L R ^c   Kennedy, John D ^c  

^a UNIVERSITY COLLEGE CORK   (Ireland)

^b UNIVERSITY OF GUELPH   (Canada)

^c UNIVERSITY OF LEEDS   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 51149216278     PISSN: 14727773     EISSN: None     Source Type: Journal    
DOI: 10.1039/DT9890001657     Document Type: Article

References (55)

1. Part 4, Faridoon, O. Ni Dhubhghaill, T. R. Spalding, G. Ferguson, B. Kaitner, X. L. R. Fontaine, J. D. Kennedy, and D. Reed, J. Chem. Soc., Dalton Trans., 1988, 2739.
2. G. Ferguson, M. Parvez, J. A. MacCurtain, O. Ni Dhubhghaill, T. R. Spalding, and D. Reed, J. Chem. Soc., Dalton Trans., 1987, 699.
3. W. R. Hertier, F. Klanberg, and E. L. Muetterties, Inorg. Chem., 1967, 6, 1696
4. A. R. Kane, L. J. Guggenberger, and E. L. Muetterties, J. Am. Chem. Soc., 1970, 92, 2571.
5. A. R. Siedle, D. McDowell, and L. J. Todd, Inorg. Chem., 1974, 13, 2735.
6. T. K. Hilty, D. A. Thompson, W. M. Butler, and R. W. Rudolph, Inorg. Chem., 1979, 18, 2642.
7. G. A. Kukina, M. A. Porai-Koshits, V. S. Sergienko, Yu. V. Zefirov, and G. G. Sadikov, Koord. Khim., 1985, 11, 385.
8. G. Ferguson, J. D. Kennedy, X. L. R. Fontaine, Faridoon, and T. R. Spalding, J. Chem. Soc., Dalton Trans., 1988, 2555.
9. Y. M. Cheek, N. N. Greenwood, J. D. Kennedy, and W. S. McDonald, J. Chem. Soc., Chem. Commun., 1982, 80.
10. A. J. Welch, J. Chem. Soc., Dalton Trans., 1975, 2270.
11. M. Green, J. L. Spencer, F. G. A. Stone, and A. J. Welch, J. Chem. Soc., Dalton Trans., 1975, 179.
12. A. J. Welch, J. Chem. Soc., Dalton Trans., 1975, 1473.
13. E. W. Corcoran and L. G. Sneddon, Inorg. Chem., 1985, 107, 7446 and refs, therein.
14. M. A. Beckett, J. D. Kennedy, and O. W. Howarth, J. Chem. Soc., Chem. Commun., 1985, 855.
15. J. D. Kennedy and B. Wrackmeyer, J. Magn. Reson., 1980, 38, 529.
16. N. N. Greenwood, M. J. Hails, J. D. Kennedy, and W. S. McDonald, J. Chem. Soc., Dalton Trans., 1985, 953.
17. S. K. Boocock, N. N. Greenwood, M. J. Hails, J. D. Kennedy, and W. S. McDonald, J. Chem. Soc., Dalton Trans., 1981, 1415.
18. J. Bould, N. N. Greenwood, and J. D. Kennedy, J. Chem. Soc., Dalton Trans., 1984, 2477.
19. J. D. Kennedy, Prog. Inorg. Chem., 1986, 34, 211 and refs, therein.
20. M. A. Beckett and J. D. Kennedy, J. Chem. Soc., Chem. Commun., 1983, 275.
21. J. D. Kennedy, in ‘Multinuclear N.M.R.,’ ed. J. Mason, Plenum, London, New York, 1987, ch. 8, pp. 221-254 and refs, therein.
22. K. Baše, A. Petrina, B. Štíbr, V. Petricek, K. Malý, A. Linek, and I. A. Zakharova, Chem. Ind. (London), 1979, 212.
23. B. Štíbr, S. Heřmánek, J. Plešek, K. Baše, and I. A. Zakharova, Chem. Ind. (London), 1980, 468.
24. D. S. Kendall and W. N. Lipscomb, Inorg. Chem., 1973, 12, 546.
25. V. R. Brill, H. Dietrick, and H. Dierks, Acta Crystallogr., Sect. B, 1971, 27, 2003.
26. G. A. Kukina, S. V. Sergienko, M. A. Porai-Koshits, K. Baše, and I. A. Zakharova, Izv. Acad. Nauk. S.S.S.R., Ser. Khim., 1981, 12, 2838.
27. G. D. Friesen, A. Barriola, D. Daluga, P. Ragatz, J. C. Huffman, and L. J. Todd, Inorg. Chem., 1980, 19, 458.
28. S. K. Boocock, J. Bould, N. N. Greenwood, J. D. Kennedy, and W. S. McDonald, J. Chem. Soc., Dalton Trans., 1982, 713.
29. M. A. Beckett, N. N. Greenwood, J. D. Kennedy, and M. Thornton-Pett, J. Chem. Soc., Dalton Trans., 1985, 1119.
30. M. J. S. Dewar and W. Thiel, J. Am. Chem. Soc., 1977, 99, 2531
31. W. Thiel, Quantum Chemistry Program Exchange, Indiana State University, Bloomington, 1978, vol. 11, p. 353.
32. N. N. Greenwood, J. A. McGinnety, and J. D. Owen, J. Chem. Soc., Dalton Trans., 1972, 986.
33. F. E. Wang, P. G. Simpson, and W. N. Lipscomb, J. Am. Chem. Soc., 1961, 83, 491.
34. T. Jelínek, B. Štíbr, F. Mares, J. Plešek, and S. Heřmánek, Polyhedron, 1987, 6, 1737.
35. K. Baše, S. Heřmánek, and F. Hanousek, J. Chem. Soc., Chem. Commun., 1984, 299.
36. G. B. Jacobsen, D. G. Meina, J. H. Morris, C. Thomson, S. J. Andrews, D. Reed, A. J. Welch, and D. F. Gaines, J. Chem. Soc., Dalton Trans., 1985, 1645.
37. J. C. Huffman and W. E. Streib, J. Chem. Soc., Chem. Commun., 1972, 665.
38. S. Heřmánek, J. Fusek, B. Štíbr, J. Plešek, and T. Jelínek, Polyhedron, 1986, 5, 1873.
39. D. G. Evans and D. M. P. Mingos, J. Organomet. Chem., 1982, 240, 321.
40. J. A. MacCurtain, P. Brint, and T. R. Spalding, J. Chem. Soc., Dalton Trans., 1985, 2591.
41. W. J. Hehre, L. Radom, P. v. R. Schleyer, and J. A. Pople, ‘Ab initio Molecular Orbital Theory,’ Wiley, New York, 1985.
42. G. W. Parshall, Inorg. Synth., 1970, 12, 27.
43. G. B. Kauffman and D. O. Cowan, Inorg. Synth., 1960, 6, 211.
44. J. L. Little, G. D. Friesen, and J. L. Todd, Inorg. Chem., 1977, 16, 869.
45. ‘International Tables for X-ray Crystallography,’ Kynoch Press, Birmingham, 1974, vol. 4.
46. SDP-Plus, B. Frenz and Associates Inc., College Station, Texas 77840, and Enraf-Nonius, Delft, 1983.
47. C.K. Johnson, ORTEP II, Report ORNL-5138, Oak Ridge National Laboratory, Tennessee, 1976.
48. X. L. R. Fontaine and J. D. Kennedy, J. Chem. Soc., Dalton Trans., 1987, 1573.
49. S. K. Boocock, N. N. Greenwood, J. D. Kennedy, W. S. McDonald, and J. Staves, J. Chem. Soc., Dalton Trans., 1981, 2573.
50. M. Bown, X. L. R. Fontaine, and J. D. Kennedy, J. Chem. Soc., Dalton Trans., 1988, 1467.
51. T. L. Venable, W. C. Hutton, and R. N. Grimes, J. Am. Chem. Soc., 1984, 106, 29.
52. X. L. R. Fontaine, H. Fowkes, N. N. Greenwood, J. D. Kennedy, and M. Thornton-Pett, J. Chem. Soc., Dalton Trans., 1987, 1431, 2417.
53. X. L. R. Fontaine and J. D. Kennedy, J. Chem. Soc., Chem. Commun., 1986, 779.
54. J. D. Kennedy and J. Staves, Z. Naturforsch., Teil B, 1979, 34, 808.
55. W. McFarlane, Proc. R. Soc. London, Ser. A, 1986, 306, 185.