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Crystal data for 3: C30H48Cl 3ErN4Ti3, Mw, 882.03, monoclinic, a, 11.177(4) Å, b, 17.907(2) Å, c, 37.753(6) Å, β, 94.39(2)°, V, 7534(3) Å3, Z, 8, space group P21/c (No. 14, T, 200(2) K, λ, 0.710 73 Å, D calcd, 1.555 g cm-3, μ, 3.055 mm-1, R1, 0.088, wR2, 0.194 [for 5909 reflections with I > 2σ(I, Crystal data for 5: C35H53Cl2ErN 4Ti3, Mw, 911.67, monoclinic, a, 11.039(4) Å, b, 18.155(6) Å, c, 19.094(6) Å, β, 94.10(2)°, V, 3817(2) Å3, Z, 4, space group P21/n (No. 14, T, 200(2) K, λ, 0.710 73 Å
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Full details of the X-ray crystal structure determination, a figure, and parameters of 6 can be found in the Supporting Information.
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Full details of the X-ray crystal structure determination, a figure, and parameters of 6 can be found in the Supporting Information.
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