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Crystal data for 1: Mr, 2738.98, 0.32 x 0.23 x 0.17 mm3, triclinic, space group, P1, a, 10.3659(16) Å, b, 16.232(2) Å, c, 20.607(3) Å, α, 104.210(3)°, β, 96.235(2)°, γ, 97.768(2)°, V, 3293.8(8) Å3, Z, 1, Dcalc, 1.381 mg/m3, 10 525 independent reflections, R1, 0.0942, wR2, 0.2132, and S, 1.004 for observed reflections with I < 2σI
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3, 10 525 independent reflections, R1 = 0.0942, wR2 = 0.2132, and S = 1.004 for observed reflections with I < 2σ(I).
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13
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