A precision apparatus, with solid phase micro-extraction monitoring capability, for incorporation studies of gaseous precursors into insect-derived metabolites

Arkivoc

Volumn 2004, Issue 10, 2004, Pages 109-117

  Fletcher, Mary T ^a   Wood, Barry J ^a   Schwartz, Brett D ^a   Rahm, Fredrik ^a   Lambert, Lynette K ^a   Brereton, Ian M ^a   Moore, Christopher J ^b   De Voss, James J ^a   Kitching, William ^a  

^a UNIVERSITY OF QUEENSLAND   (Australia)

^b DEPARTMENT OF AGRICULTURE AND FISHERIES   (Australia)

Author keywords

18O labelling; Carbon monoxide; Carbon 13 NMR spectra; Incorporation studies; Insect chamber; Isotope effects; Metabolites; Spiroacetals

Indexed keywords

CARBON 13; DECANE; ISOTOPE; OXYGEN 18;

ACCURACY; ANALYTIC METHOD; APPARATUS; ARTICLE; DROSOPHILA; GAS ANALYSIS; LIQUID PHASE MICROEXTRACTION; METABOLITE; MIGRATION; NONHUMAN; PRESSURE CHAMBER; PROTON NUCLEAR MAGNETIC RESONANCE; SOLID; SPECIES IDENTIFICATION; WASP;

EID: 5044238111     PISSN: 14246376     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (13)

1. Hungerford, N.L.; Mazomenos, B.E.; Konstantopoulou, M.A.; Krolcos, F.D.; Haniotakis, G.E.; Hübener, A.; Fletcher, M.T.; Moore, C.J; Kitching, W. Chem. Commun. 1998, 863.
2. Stok, J.E.; Lang, C-S.; Schwartz, B.D.; Fletcher, M.T.; Kitching, W.; De Voss, J.J. Org. Lett. 2001, 3, 397.
3. (a) Fletcher, M.T.; Wood, B.J.; Brereton, I.M.; Stok, J.E.; De Voss, J.J.; Kitching, W. J. Am. Chem. Soc. 2002, 124, 7666.
4. (b) Fletcher, M.T.; Mazomenos, B.E.; Georgakopoulos, J.H.; Konstantopoulou, M.A.; Wood, B.J.; De Voss, J.J.; Kitching, W. Chem. Commun. 2002, 1302.
5. McErlean, C.S.P.; Fletcher M.T.; Wood, B.J.; De Voss, J.J.; Kitching, W. Org. Lett. 2002, 4, 2775.
6. Fletcher, M.T.; Kitching, W. Chem. Rev. 1995, 95, 789.
7. Francke, W.; Kitching, W. Curr. Org. Chem. 2001, 5, 233.
8. nd ed.; Plenum Press: New York, 1995.
9. Davies, N.W.; Madden, J.L. J. Chem. Ecol. 1985, 11, 1115. See also Forest and Timber Insects in New Zealand No. 47 - Insect Parasites of Sirex (http://www.forestresearch.co.nz).
10. Davies, N.W.; Madden, J.L. J. Chem. Ecol. 1985, 11, 1115. See also Forest and Timber Insects in New Zealand No. 47 - Insect Parasites of Sirex (http://www.forestresearch.co.nz).
11. 18O]) was manufactured by Yeda R & D Co. Ltd, Israel. A Carboxen PDMS fibre (Supelco) was employed.
12. 2]-dioxygen atmosphere are reproduced in ref. 3(b).
13. For some discussion of oxygen-atom exchange between dioxygen and water see footnote 13 in Vanderwel, D.; Oehlschlager, A.C. J. Am. Chem. Soc. 1992, 114, 5081.