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note
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2).
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40
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50249158782
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note
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int = 0.1092). R = 0.040 and wR = 0.101, GOF = 0.983 for 337 parameters. The intensity data were measured on a Bruker Smart CCD diffractomerter with graphite-monochromated Mo Kα (λ = 0.7107 Å) at 296(2) K. Empirical absorption corrections were applied using the SADABS program. All calculations were performed using the SHELXL-97 program package [34]. The structure was solved by direct methods and refined by full-matrix least-squares methods. All non-hydrogen atoms were refined anisotropically, while all hydrogen atoms were located from differential Fourier maps.
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