Enantioselective determination of alprenolol in human plasma by liquid chromatography with tandem mass spectrometry using cellobiohydrolase chiral stationary phases

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 872, Issue 1-2, 2008, Pages 121-127

  Jiang, Hongliang ^a   Jiang, Xiangyu ^a   Ji, Qin C ^a  

^a Late Stage Developmental Services Covance Inc   (United States)

Author keywords

Alprenolol; Cellobiohydrolase (CBH); Chiral separation; LC MS MS; Supported liquid extraction (SLE)

Indexed keywords

CHIRALITY; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; CONCENTRATION (PROCESS); CUSTOMER SATISFACTION; ENANTIOMERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PHASE SEPARATION; PLASMA (HUMAN); PLASMAS; PROBLEM SOLVING; QUALITY ASSURANCE; QUALITY FUNCTION DEPLOYMENT; SEPARATION; SOLVENT EXTRACTION; STANDARDS; TOTAL QUALITY MANAGEMENT;

96-WELL; ALPRENOLOL; BASELINE SEPARATION; BIOANALYTICAL METHODS; CELLOBIOHYDROLASE; CELLOBIOHYDROLASE (CBH); CHIRAL SEPARATION; CHIRAL STATIONARY PHASES; CONTROL SAMPLES; DIRECT DETERMINATION; ENANTIOSELECTIVE; H IGH CONCENTRATIONS; HUMAN PLASMAS; LC-MS/MS; LIQUID EXTRACTION; METHOD VALIDATIONS; PLASMA SAMPLES; RELATIVE ERROR; RELATIVE STANDARD DEVIATION; REVERSED PHASE CHROMATOGRAPHY; SAMPLE EXTRACTION; SUPPORTED LIQUID EXTRACTION (SLE); TANDEM MASS SPECTROMETRY;

EXTRACTION;

ALPRENOLOL;

ACCURACY; ARTICLE; CONCENTRATION (PARAMETERS); ENANTIOMER; ENANTIOSELECTIVITY; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; QUALITY CONTROL; TANDEM MASS SPECTROMETRY;

ADRENERGIC BETA-ANTAGONISTS; ALPRENOLOL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; STEREOISOMERISM; TANDEM MASS SPECTROMETRY;

EID: 49849096962     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2008.07.022     Document Type: Article

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