Solvent-free wittig reaction: A green organic chemistry laboratory experiment

Journal of Chemical Education

Volumn 81, Issue 10, 2004, Pages 1492-1493

  Leung, Sam H ^a   Angel, Stephen A ^a  

^a WASHBURN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AROMATIC COMPOUNDS; BROMINE COMPOUNDS; CHLORINE COMPOUNDS; COMPOSITION EFFECTS; CRYSTALLIZATION; ETHANOL; EXPERIMENTS; POTASSIUM COMPOUNDS; SYNTHESIS (CHEMICAL); TEACHING; WASHING;

BENZYLTRIPHENYLPHOSPHONIUM CHLORIDE; BROMOBENZALDEHYDE; BROMOPHENYL PHENYLETHENE; GREEN ORGANIC CHEMISTRY; LABORATORY EXPERIMENT; POTASSIUM PHOSPHATE; SELVENT FREE WITTIG REACTION;

CHEMISTRY;

EID: 4944251314     PISSN: 00219584     EISSN: None     Source Type: Journal    
DOI: 10.1021/ed081p1492     Document Type: Article

References (24)

1. Cox, C. F. Experimental Organic Chemistry; Macmillan: New York, 1988; pp 301-304.
2. Pavia, D. L.; Lampman, G. M.; Kriz, G. S.; Engel, R. G. Introduction to Orgnanic Laboratory Techniques; Saunders: Philadelphia, PA, 1990; pp 297-302.
3. Nimitz, J. S. Experiments in Organic Chemistry; Prentice Hall: Englewood Cliffs, NJ, 1991; pp 291-294.
4. Mayo, D. W.; Pike, R. M.; Trumper, P. K. Microscale Organic Laboratory, 3rd ed.; Wiley: New York, 1994; pp 297-313.
5. Mohrig, J. R.; Hammond, C. N.; Morrill, T. C.; Neckers, D. C. Experimental Organic Chemistry; Freeman: New York, 1998; pp 267-274.
6. Williamson, K. L. Macroscale and Microscale Organic Experiments, 3rd ed.; Houghton Mifflin: Boston, MA, 1999; pp 464-470.
7. Lehman, J. W. Operational Organic Chemistry, 3rd ed.; Prentice Hall: Upper Saddle River, NJ, 1999; pp 315-322.
8. Broos, R.; Tavernier, D.; Anteunis, M. J. Chem. Educ. 1978, 55, 813.
9. Gillois, J.; Guillerm, G.; Savignac, M.; Stephan, E.; Vo-Quang, L. J. Chem. Educ. 1980, 57, 161-162.
10. Lampman, G. M.; Koops, R. W.; Olden, C. C. J. Chem. Educ. 1985, 62, 267-268.
11. Warner, J. C.; Anastas, P. T.; Anselme J.-P. J. Chem. Educ. 1985, 62, 346.
12. Silversmith, E. F. J. Chem. Educ. 1986, 63, 645.
13. Pike, R. M.; Mayo, D. W.; Butcher, S. S.; Butcher, D. J.; Hinkle, R. J. J. Chem. Educ. 1986, 63, 917-918.
14. Breuer, S. W. J. Chem. Educ. 1991, 68, A58-A60.
15. Breton, G. W. J. Chem. Educ. 1997, 74, 114-115.
16. Jaworek, C.; Iacobucci, S. J. Chem. Educ. 2002, 79, 111.
17. Singh, M. M.; Szafran, Zvi; Pike, R. M. J. Chem. Educ. 1999, 76, 1684-1686.
18. Hjeresen, D. L.; Shutt, D. L.; Boese, J. M. J. Chem. Educ. 2000, 77, 1543-1547.
19. Kirchhoff, M. M. J. Chem. Educ. 2001, 78, 1577.
20. Reed, S. M.; Hutchison, J. E. J. Chem. Educ. 2000, 77, 1627-1629.
21. Pohl, N.; Clague, A.; Schwarz, K. J. Chem. Educ. 2002, 79, 727-728.
22. Harper, B. A., Rainwater, J. C.; Birdwhistell, K.; Knight, D. A. J. Chem. Educ. 2002, 79, 729-731.
23. Palleros, D. R. J. Chem. Educ. 2004, 81, 1345-1347.
24. Balema, V. P.; Wiench, J. W.; Pruski, M.; Pecharsky, V. K. J. Am. Chem. Soc. 2002, 124, 6244-6245.