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Tetrahedron Letters

Volumn 17, Issue 21, 1976, Pages 1831-1834

Catalytic asymmetric induction in oxidation reactions. The synthesis of optically active epoxides.

(5) Helder, R a Hummelen, J C a Laane, R W P M a Wiering, J S a Wynberg, Hans a

a UNIVERSITY OF GRONINGEN (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 49349138832 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)93796-1 Document Type: Article

Times cited : (212)

References (29)

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26
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- Great care was exercised to remove all of the catalyst and its degradation fragments from the product. Duplicate and blank experiments were performed. Experiments were carried out to ensure that the optical activity of the epoxides was not due to fortuitous resolution in the presence of the catalyst.

27
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- Optically active epoxides had analytical and/or spectral data in accord with their structure and with those reported for the known racemic substances.

28
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- This experiment was separately carried out on (−), (+) and racemic samples of epoxide 6b and proves that the enantiomers of 6b were indeed formed in different amounts.

29
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- For the enantioselective addition of thiols to electron-poor double bonds, see R. Helder, R. Arends and H. Wynberg, manuscript in preparation.

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