Improved and facile addition reactions of pentafluorosulfanyl bromide

Tetrahedron Letters

Volumn 49, Issue 39, 2008, Pages 5662-5663

  Lim, Dong Sung ^a   Ngo, Silvana C ^a   Lal, Sankar G ^b   Minnich, Kristen E ^b   Welch, John T ^a  

^a STATE UNIVERSITY OF NEW YORK   (United States)

^b AIR PRODUCTS AND CHEMICALS INC   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ALKENE; SULFONE DERIVATIVE;

ADDITION REACTION; ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; FLUORINE NUCLEAR MAGNETIC RESONANCE; SYNTHESIS;

EID: 49149097784     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2008.07.080     Document Type: Article

References (15)

1. Kovacina, T. A.; DeMarco, R. A.; Snow, A. W. US Patent 4,535,011, 1985.
2. Winter R., and Gard G.L. J. Fluorine Chem. 102 (2000) 79-87
3. Winter R., and Gard G.L. J. Fluorine Chem. 107 (2001) 23-30
4. Winter R.W., Dodean R., Holmes L., and Gard G.L. J. Fluorine Chem. 125 (2004) 37-41
5. Winter R.W., and Gard G.L. J. Fluorine Chem. 125 (2004) 549-552
6. Samia A., and Dolbier W.R. Org. Lett. 4 (2002) 3013-3015
7. Tatina A.S., and Dolbier W.R. Org. Lett. 6 (2004) 2417-2419
8. Dolbier W.R., Ait-Mohand S., Schertz T.D., Sergeeva T.A., Cradlebaugh J.A., Mitani A., Gard G.L., Winter R.W., and Thrasher J.S. J. Fluorine Chem. 127 (2006) 1302-1310
9. Dolbier W.R., Mitani A., and Warren R.D. Tetrahedron Lett. 48 (2007) 1325-1326
10. Lal, G. S.; Minnich, K. E. Patent US 6,479,645, 2002.
11. Lal, G. S.; Minnich, K. E. Patent US 6,870,068, 2005.
12. 4 and concentrated. The crude product was purified by Kügelrohr distillation or flash chromatography to afford the liquid, colorless product in good yield.
13. 4), and filtered.
14. 4 and concentrated in vacuo. The crude product was purified by flash chromatography to afford the colorless liquid product in good yield.
15. Smith M.B., and March J. March's Advanced Organic Chemistry (2007), Wiley-Interscience, Hoboken, NJ