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49049118610
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Selected physical and spectroscopic data for compound 5c: Red powder (0.400 g, 95, mp 232-235°C; FT-IR (KBr, νmax, cm-1, 3250 (N-H, 1635 (C=O, δH (400.1 MHz, CDCl3) 1.32-2.34 (10H, m, 5 CH2, 3.95 (1H, m, N-CH, 7.14 (1H, d, J 7.3 Hz, NH, 7.39-8.48 (11H, m, arom. hydrogens, δC (100.7 MHz, CDCl3) 190.24, 178.61, 164.72, 150.57, 141.31, 134.50, 131.90, 131.04, 130.94, 130.28, 130.16, 129.04, 128.52, 128.23, 127.44, 126.85, 126.30, 124.33, 122.63, 120.17, 119.86, 95.02, 51.75, 33.37, 25.41, 24.52; Anal. Calcd. for C28H23NO 3 (421.48, C, 79.79; H, 5.50; N, 3.32, Found: C, 79.70; H, 5.53; N, 3.40, Selected physical and spectroscopic data for compound 5h: Purple powder (0.404 g, 92, mp 195-197°C; FT-IR (KBr, νmax, cm-1, 3427 (N-H, 1618 (C=O, δH 400.1 MHz, CDCl
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4 (438.47): C, 73.96; H, 5.06; N, 6.39%. Found: C, 74.04; H, 5.07; N, 6.22%.
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