A multiresidue method for the analysis of carbamate and urea pesticides from soils by microwave-assisted extraction and liquid chromatography with photodiode array detection

Analytical Letters

Volumn 41, Issue 10, 2008, Pages 1751-1772

  Paíga, Paula ^a   Morais, Simone ^a   Correia, Manuela ^a   Alves, Arminda ^b   Delerue Matos, Cristina ^a  

^a INSTITUTO SUPERIOR DE ENGENHARIA DO PORTO   (Portugal)

^b UNIVERSITY OF PORTO   (Portugal)

Author keywords

Carbamates; Liquid chromatography; Microwave assisted extraction; Pesticides; Soils; Ureas

Indexed keywords

EID: 48749088832     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032710802162392     Document Type: Article

References (37)

1. http://www.dgpc.min-agricultura.pt (October 2007).
2. Ahmad, I. and Crawford, G. 1990. Trace residue analysis of the herbicide chlorsulfuron in soil by gas chromatography-electron capture detection. J. Agric. Food Chem., 38: 138-141.
3. Barnabas, I.J., Dean, J.R., Fowlis, I.A., and Owen, S.P. 1995. Extraction of polycyclic aromatic-hydrocarbons from highly contaminated soils using microwave-energy. Analyst, 120: 1897-1904.
4. Berrada, H., Font, G., and Moltó, J.C. 2003. Determination of urea pesticide residue in vegetable, soil, and water samples. Anal. Chem., 33: 19-41.
5. Blanco, E.V., Mahia, P.L., Lorenzo, S.M., and Rodriguez, D.P. 2000. Optimization of microwave-assisted extraction of hydrocarbons in marine sediments: comparison with the soxhlet extraction method. Fresenius J. Anal. Chem., 366: 283-288.
6. Bouaid, A., Martin-Esteban, A., Fernández, P., and Cámara, C. 2000. Microwave-assisted extraction method for the determination of atrazine and four organophosphorus pesticides in oranges by gas chromatography (GC). Fresenius J. Anal. Chem., 367: 291-294.
7. Carabias-Martinez, R., Rodríguez-Gonzalo, E., Herrero- Hernández, E., and Hernández-Méndez, J. 2004. Simultaneous determination of phenyl- and sulfonylurea herbicides in water by solid-phase extraction and liquid chromatography with UV diode array or mass spectrometric detection. Anal. Chim. Acta., 517: 71-79.
8. Chee, K.K., Wong, M.K., and Lee, H.K. 1996. Optimization of microwave-assisted solvent extraction of polycyclic aromatic hydrocarbons in marine sediments using a microwave extraction system with high-performance liquid chromatography fluorescence detection and gas chromatography mass spectrometry. J. Chromatogr. A, 723: 259-271.
9. de la Huebra, M.J.G., Hernández, P., Ballesteros, Y., and Hernández, L. 2001. Determination of linuron in soil by stripping voltammetry with carbon fiber microelectrode. Talanta, 54: 1077-1085.
10. de Sabando, O.L., de Balugera, Z.G., Goicolea, M.A., Rodriguez, E., Sampedro, M.C., and Barrio, R.J. 2002. Determination of simazine and cymoxanil in soils by microwave-assisted solvent extraction and HPLC with reductive amperometrical detection. Chromatographia, 55: 667-671.
11. Font, N., Hernández, F., Hogendoorn, E.A., Baumannb, R.A., and Van Zoonenb, P. 1998. Microwave-assisted solvent extraction and reversed-phase liquid chromatography-UV detection for screening soils for sulfonylurea herbicides. J. Chromatogr. A, 798: 179-186.
12. Hesse, P.R., ed. 1972. A Textbook of Soil Chemical Analysis. New York: Chemical Publishing Co., Inc.
13. Herbert, P., Morais, S., Paíga, P., Alves, A., and Santos, L. 2006a. Analysis of PCBs in soils and sediments by microwave-assisted extraction, headspace-SPME and high resolution gas chromatography with ion-trap tandem mass spectrometry. Intern. J. Environ. Anal. Chem., 86: 391-400.
14. Herbert, P., Morais, S., Paíga, P., Alves, A., and Santos, L. 2006b. Development and validation of a novel method for the analysis of chlorinated pesticides in soils using microwave-assisted extraction-headspace solid phase microextraction and gas chromatography-tandem mass spectrometry. Anal. Bioanal. Chem., 384: 810-816.
15. Jan, M.R., Shah, J., and Khan, H. 2003. Investigation of new indirect spectrophotometric method for the determination of carbofuran in carbamate pesticides. Chemosphere, 52:1623-1626.
16. Laganà, A., Fagoa, G., Marino, A., and Penazzi, V.M. 2000. Liquid chromatography mass spectrometry tandem for multiresidue determination of selected post-emergence herbicides after soil column extraction. Anal. Chim. Acta, 415: 41-56.
17. Lopez-Avila, V., Richard, Y., and Werner, F.B. 1994. Microwave-assisted extraction of organic compounds from standard reference soils and sediments. Anal. Chem., 66: 1097-1106.
18. Lopez-Avila, V., Richard, Y., Benedicto, J., Ho, P., Kim, R., and Beckert, F.B. 1995. Extraction of organic pollutants from solid samples using microwave energy. Anal. Chem., 67: 2096-2102.
19. Macutkewicz, E., Rompa, M., and Zygmunt, B. 2003. Sample preparation and chromatographic analysis of acidic herbicides in soils and sediments. Critical Reviews in Anal Chem., 33: 1-17.
20. Miller, J.C. and Miller, J.N. eds. 1994. Statistical far Analytical Chemistry. New York: Ellis Horwood Limited.
21. Molins, C., Hogendoorn, E.A., Heusinkveld, H.A.G., Vanharten, D.C., Vanzoonen, P., and Baumann, R.A. 1996. Microwave assisted solvent extraction (MASE) for the efficient determination of triazdnes in soil samples with aged residues. Chromatographia, 43: 527-532.
22. Molins, C., Hogendoorn, E.A., Heusinkveld, H.A.G., Van Zoonen, P., and Baumann, R.A. 1997. Microwave-assisted solvent extraction (MASE) of organochlorine pesticides from soil samples. Intern. J. Environ. Anal. Chem., 68: 155-169.
23. Molins, C., Hogendoorn, E.A., Dijkman, E., Heusinkveld, H.A.G., and Baumann, R.A. 2000. Determination of linuron and related compounds in soil by microwave-assisted solvent extraction and reversed phase liquid chromatography with UV detection. J. Chromatogr. A, 896: 487-496.
24. Morais, S., Tavares, O., Baptista-Paíga, P.C., and Delerue-Matos, C. 2004. Anodic adsorptive stripping voltammetric determination of atraztne in spiked soil samples with a gold microelectrode. Anal. Lett., 37: 3271-3286.
25. Prados-Rosales, R.C., Herrera, M.C., Luque-García, J.L., and de Castro, M.D.L. 2002. Study of the feasibility of focused microwave-assisted soxhlet extraction of N-methylcarbamates in soil. J. Chromatogr. A, 953: 133-140.
26. Srogi, K. 2006. A review: Application of microwave techniques for environmental analytical chemistry. Anal. Lett., 39: 1261-1288.
27. Steinheimer, T.R. 1993. HPLC determination of atrazine and principal degradates in agricultural soils and associated surface and ground-water. J. Agric. Food Chem., 41: 588-595.
28. Sun, L. and Lee, H.K. 2002. Microwave-assisted extraction behaviour of nonpolar and polar pollutants in soil with analysis by high-performance liquid chromatography. J. Sep. Sci., 25: 67-76.
29. Sun, L. and Lee, H.K. 2003a. Stability studies of propoxur herbicides in environmental water samples by liquid chromatography-atmospheric pressure chemical ionization ion-trap mass spectrotmetry. J. Chromatogr. A., 1014: 153-163.
30. Sun, L. and Lee, H.K. 2003b. Optimization of microwave-assisted extraction and supercritical fluid extraction of carbamate pesticides in soil by experimental design methodology. J. Chromatogr. A, 1014: 165-177.
31. Tavares, O., Morais, S., Paiga, P., and Delerue-Matos, C. 2005. Determination of ametryn in soils via microwave-assisted solvent extraction coupled to anodic stripping voltammetry with a gold ultramicroelectrode. Anal. Bioanal. Chem., 382: 477-484.
32. Tomlin, C.D.S., eds. 1997. The Pesticide Manual, 11th ed. Surrey, UK: British Crop Protection Council.
33. U.S. Environmental Protection Agency. 1994. EPA Method 8318. N-Methylcarbamates by High Performance Liquid Chromatography. Washington, DC.
34. U.S. Environmental Protection Agency. 2000. EPA Method 3546. Microwave Extraction of VOCs and SVOCs organophosphorus pesticides, organochlorine pesticides, chlorinated herbicides, phenoxy acid herbicides, PCBs. Cincinnati, OH: U.S. Environmental Protection Agency, Office of Research and Development, National Exposure Research Laboratory.
35. Vryzas, Z. and Papadopoulou-Mourkidou, E. 2002. Determination of triazine and chloroacetanilide herbicides in soils by microwave-assisted extraction (MAE) coupled to gas chromatographic analysis with either GC-NPD or GC-MS. J. Agric. Food Chem., 50: 5026-5033.
36. Xiong, G., Hebm, X., and Zhang, Z. 2000. Microwave-assisted extraction or saponification combined with microwave-assisted decomposition applied in pretreatment of soil or mussel samples for the determination of polychlorinated biphenyls. Anal. Chim. Acta., 413: 49-56.
37. Zahnow, E.W. 1985. Analysis of the herbicide sulfometuron methyl in fish and green plants by liquid-chromatography. J. Agric. Food Chem., 33: 1206-1208.