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Volumn 49, Issue 38, 2008, Pages 5505-5507

N-Amino-endo-bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide in reaction of oxidative aminoaziridination

Author keywords

[No Author keywords available]

Indexed keywords

ALKENE DERIVATIVE; AZIRIDINE DERIVATIVE; BENZENE DERIVATIVE; N AMINO ENDO BICYCLO[2.2.1]HEPT 5 ENE 2,3 DICARBOXIMIDE;

EID: 48549092387     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2008.07.046     Document Type: Article
Times cited : (12)

References (31)
  • 24
    • 48549107905 scopus 로고    scopus 로고
    • note
    • 2 were added simultaneously dropwise to the reaction mixture over 10 min. The mixture was stirred at -78 °C for 30 min and then warmed to room temperature and stirred for 10 min. The resulting solution was filtered through a short plug of silica gel, solvent was removed on rotary evaporator without heating and the residue was triturated with 15 mL of diethyl ether. If no crystallization occurred, the crude product was purified by column chromatography (silica gel, ethyl acetate/hexane 1:1). Recrystallization of the product from methanol was necessary in some cases.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.