Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals

Ceramics International

Volumn 34, Issue 7, 2008, Pages 1691-1695

  Thongtem, Titipun ^a   Kaowphong, Sulawan ^a   Thongtem, Somchai ^a  

^a CHIANG MAI UNIVERSITY   (Thailand)

Author keywords

Hydrothermal synthesis; l Cysteine; N Cetyl pyridinium chloride; PbS crystals

Indexed keywords

CRYSTALLOGRAPHY; CRYSTALS; LEAD; POWDERS; SURFACE ACTIVE AGENTS; SYNTHESIS (CHEMICAL);

HYDROTHERMALLY SYNTHESIZED; L-CYSTEINE; N-CETYL PYRIDINIUM CHLORIDE; PBS CRYSTALS;

HYDROTHERMAL SYNTHESIS;

EID: 48349116217     PISSN: 02728842     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ceramint.2007.05.007     Document Type: Article

References (19)

1. 4 nanocrystal and its phase transition to PbS. Mater. Lett. 59 (2005) 3507-3513
2. Xu L., Zhang W., Ding Y., Yu W., Xing J., Li F., and Qian Y. Shape-controlled synthesis of PbS microcrystals in large yields via a solvothermal process. J. Cryst. Growth 273 (2004) 213-219
3. Zhang Y.C., Qiao T., Hu X.Y., Wang G.Y., and Wu X. Shape-controlled synthesis of PbS microcrystallites by mild solvothermal decomposition of a single-source molecular precursor. J. Cryst. Growth 277 (2005) 518-523
4. Wang S., Pan A., Yin H., He Y., Lei Y., Xu Z., and Zou B. Synthesis of PbS microcrystals via a hydrothermal process. Mater. Lett. 60 (2006) 1242-1246
5. Qin A.M., Fang Y.P., Zhao W.X., Liu H.Q., and Su C.Y. Directionally dendritic growth of metal chalcogenide crystals via mild template-free solvothermal method. J. Cryst. Growth 283 (2005) 230-241
6. Wang S.F., Gu F., Lü M.K., Wang D.Z., Yang Z.S., Zhang H.P., Zhou Y.Y., and Zhang A.Y. Synthesis of cross-shaped PbS nanostructures by a surfactant-assisted reflux process. Mater. Lett. 60 (2006) 2759-2763
7. Zhou G., Lü M., Xiu Z., Wang S., Zhang H., Zhou Y., and Wang S. Controlled synthesis of high-quality PbS star-shaped dendrites, multipods, truncated nanocubes, and nanocubes and their shape evolution process. J. Phys. Chem. B 110 (2006) 6543-6548
8. Ni Y., Wang F., Liu H., Yin G., Hong J., Ma X., and Xu Z. A novel aqueous-phase route to prepare flower-shaped PbS micron crystals. J. Cryst. Growth 262 (2004) 399-402
9. Dong L., Chu Y., Liu Y., Li M., Yang F., and Li L. Surfactant-assisted fabrication PbS nanorods, nanobelts, nanovelvet-flowers and dendritic nanostructures at lower temperature in aqueous solution. J. Colloid Interf. Sci. 301 (2006) 503-510
10. Chen X., Zhang X., Wang Z., Wan J., and Qian Y. Biomolecule-assisted hydrothermal synthesis and one-dimensional self-assembly of copper sulfide nanocrystallites. Mater. Chem. Phys. 98 (2006) 419-421
11. Chen X., Zhang X., Shi C., Li X., and Qian Y. A simple biomolecule-assisted hydrothermal approach to antimony sulfide nanowires. Solid State Commun. 134 (2005) 613-615
12. Powder Diffract. File, JCPDS Int. Centre Diffract. Data, PA 19073-3273, USA, 2001.
13. 12 powder prepared by the citrate and oxalate coprecipitation processes. Ceram. Int. 30 (2004) 1463-1470
14. 2 using malonic acid as a chelating agent. Ceram. Int. 31 (2005) 241-247
15. 2 prepared using succinic acid as a complexing agent. Inorg. Mater. 42 (2006) 202-209
16. Andrews K.W., Dyson D.J., and Keown S.R. Interpretation of Electron Diffraction Patterns. second ed. (1971), Plenum Press, NY
17. Cullity B.D. Elements of X-ray Diffraction. second ed. (1978), Addison-Wesley Publ. Co., MA
18. Smith G.D., Firth S., Clark R.J.H., and Cardona M. First- and second-order Raman spectra of galena (PbS). J. Appl. Phys. 92 (2002) 4375-4380
19. Alonso M., and Finn E.J. Fundamental University Physics vol. 3 (1968), Addison-Wesley Publ. Co., MA