Simplified method for determination of clarithromycin in human plasma using protein precipitation in a 96-well format and liquid chromatography-tandem mass spectrometry

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 871, Issue 1, 2008, Pages 130-134

  Shin, Jaekyu ^a,b   Pauly, Daniel F ^c   Johnson, Julie A ^a,b,c   Frye, Reginald F ^a,b  

^a UNIVERSITY OF FLORIDA HEALTH   (United States)

^b UNIVERSITY OF FLORIDA   (United States)

^c UNIVERSITY OF FLORIDA COLLEGE OF MEDICINE   (United States)

Author keywords

Clarithromycin; Human plasma; LC MS; Protein precipitation; Roxithromycin

Indexed keywords

ACETONITRILE; AMMONIUM COMPOUNDS; BODY FLUIDS; CARBOXYLIC ACIDS; CENTRIFUGATION; CHEMICALS; CHROMATOGRAPHIC ANALYSIS; FLUIDS; FORMIC ACID; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; INJECTION (OIL WELLS); LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS; MASS SPECTROMETRY; METHANOL; MIXING; OFFSHORE OIL WELL PRODUCTION; ORGANIC ACIDS; PLASMA (HUMAN); PLASMAS; RATE CONSTANTS; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS; STANDARDS;

(4-NITROPHENYL) ACETONITRILE; 96 WELL; AMMONIUM ACETATE; ANALYTES; CLARITHROMYCIN (CLM); ELSEVIER (CO); HEALTHY SUBJECTS; HUMAN PLASMA SAMPLES; HUMAN PLASMAS; INTERNAL STANDARD (IS); ION ELECTROSPRAY; LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY (LC MS MS); MOBILE PHASE; PHARMACOKINETIC STUDIES; PLASMA PROTEINS; PROTEIN PRECIPITATION; ROXITHROMYCIN; RUN TIME; SELECTED REACTION MONITORING (SRM); SIMPLIFIED METHOD; SUPERNATANTS; VORTEX MIXING;

CHROMATOGRAPHY;

ACETONITRILE; AMMONIUM ACETATE; CLARITHROMYCIN; FORMIC ACID; METHANOL; PLASMA PROTEIN; ROXITHROMYCIN; WATER;

ACCURACY; ARTICLE; BLOOD SAMPLING; CENTRIFUGATION; DRUG BLOOD LEVEL; DRUG DETERMINATION; FLOW RATE; HUMAN; INJECTION; LIQUID CHROMATOGRAPHY; MONITORING; POSITIVE ION ELECTROSPRAY; PRECIPITATION; PRIORITY JOURNAL; STANDARD; SUPERNATANT; TANDEM MASS SPECTROMETRY; TIME; VALIDATION STUDY;

CHROMATOGRAPHY, LIQUID; CLARITHROMYCIN; HUMANS; PRECIPITATION; REPRODUCIBILITY OF RESULTS; TANDEM MASS SPECTROMETRY;

EID: 48049114188     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2008.06.050     Document Type: Article

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