New rapid validated HPTLC method for the determination of galanthamine in Amaryllidaceae plant extracts

Phytochemical Analysis

Volumn 19, Issue 4, 2008, Pages 353-358

  Abou Donia, Amina H ^a   Toaima, Soad M ^a   Hammoda, Hala M ^a   Shawky, Eman ^a  

^a Alexandria University Faculty of Pharmacy   (Egypt)

Author keywords

Amaryllidaceae; Analysis; Galanthamine; HPTLC; Narcissus cv. Breath of Spring

Indexed keywords

AMARYLLIDACEAE; ANALYSE; BREATH OF SPRING; GALANTHAMINE; HPTLC; NARCISSU CV.;

PLANT EXTRACTS;

AMARYLLIDACEAE ALKALOID; GALANTAMINE;

ACCURACY; ARTICLE; CHEMICAL REACTION; CONTROLLED STUDY; DRUG DETERMINATION; HIGH PERFORMANCE THIN LAYER CHROMATOGRAPHY; NARCISSUS; NONHUMAN; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; VALIDATION STUDY;

AMARYLLIDACEAE; NARCISSUS;

EID: 48049111770     PISSN: 09580344     EISSN: 10991565     Source Type: Journal    
DOI: 10.1002/pca.1061     Document Type: Article

References (26)

1. Ansari MJ, Ahmad S, Kohli K, Ali J, Khar RK. 2005. Stability-indicating HPTLC determination of curcumin in bulk drug and pharmaceutical formulations. J Pharm Biomed Anal 39: 132-138.
2. Bastida J, Llabre's JM, Viladomat F, Codina C, Rubiralta M, Feliz M. 1987a Narcissus alkaloids, III. 9-O-Demethylhomolycorine from Narcissus confusus. J Nat Prod 50: 199.
3. Bastida J, Viladomat F, Llabre's JM, Codina C, Feliz M, Rubiralta M. 1987b. Alkaloids from Narcissus confusus. Phytochemistry 26: 1519.
4. Bastos JK, Xu L., Nanayakkara NPD, Burandt CL, Moraes-Cerdeira RM, McChesney JD. 1996. A rapid quantitative method for the analysis of galanthamine and other Amaryllidaceae alkaloids by capillary column gas chromatography. J Nat Prod 59: 638-640.
5. Cherkasov OA, Tolkachev ON. 2002. Narcissus and daffodil: the genus Narcissus. In Medicinal and Aromatic Plants - Industrial Profiles, Vol. 21. Hanks GR (ed). Taylor & Francis: London; 242.
6. Claessens HA, Thiel MV, Westra P, Soeterboek AM. 1983. High-performance liquid chromatographic determination of galanthamine, a long acting anticholinesterase drug, in serum, urine, and bile. J Chromatogr 275: 345-353.
7. Harborne JB, Baxter H. (editors) 1993. Amaryllidaceae alkaloids. In Phytochemical Dictionary. Taylor & Francis: London; 129.
8. Harvey AL. 1995. The pharmacology of galanthamine ad its analogues. Pharm Ther 68: 119-128.
9. Hoshino O. 1998. The amaryllidaceae alkaloids. In The Alkaloids, Chemistry and Biology, Vol. 51, Cordell GA (ed). Academic Press: San Diego, CA; 324-342.
10. ICH 1995a. ICH Guidelines Q 2A. Validation of Analytical Procedures: Definition and Terminology (CPMP/ICH/381/95).
11. ICH 1995b. ICH Guidelines Q 2B, Validation of Analytical Procedures: Methodology (CPMP/ICH/281/95).
12. Kewitz H. 1996. Galanthamine. A viewpoint. Drug Aging 9: 66-67.
13. Kreh M. 2002. Narcissus and daffodil: the genus Narcissus. In Medicinal and Aromatic Plants - Industrial Profiles, Vol. 21, Hanks GR (ed). Taylor & Francis: London; 256.
14. Lopez S, Bastida J, Viladomat F, Codina C. 2002. Solid-phase extraction and reversed-phase high-performance liquid chromatography of the five major alkaloids in Narcissus confusus. Phytochem Anal 13: 311-315.
15. Lopez S, Bastida J, Viladomat F, Codina C. 2003. Galanthamine pattern in Narcissus confusus plants. Planta Med 69: 1166.
16. Luttmann E, Linnemann E, Fels G. 2002. Galanthamine as a bisfunctional ligand for the acetylcholinesterase. J Mol Model 8: 208-216.
17. Marcy JB, Kinghorn A. 2005. Drug discovery from medicinal plants. Life Sci 78: 431-441.
18. Mustafa NR, Rhee IK, Verpoorte R. 2003. Rapid method for determination of galanthamine in Amaryllidaceae plants using HPLC. J Liq Chromatogr Relat Technol 26: 3217-3233.
19. Nordberg A, Svensson AL. 1998. Cholinesterase inhibitors in the treatment of Alzheimer's disease. A comparison of tolerability and pharmacology. Drug Safety 19: 465-480.
20. Obreshkova D, Pangarova T, Lazarova V. 2000. HPLC determination of galanthamine and related alkaloids in nivalin. Dokl Bulg Akad Nauk 53: 51-52.
21. Orhan BS. 2000. Sustainable use of various Amaryllidaceae plants against Alzheimer's disease. ISHS Acta Horticulturae 678: III WOCMAP Congress on Medicinal and Aromatic Plants, Vol 4: Targeted Screening of Medicinal and Aromatic Plants, Economics and Law.
22. Poulev A, Neumann BD, Zenk MH. 1993. Enzyme immunoassay for the quantitative determination of galanthamine. Planta Med 59: 442-446.
23. Selles M, Bastida J, Viladomat F, Codina C. 1997. Quantitative evaluation of galanthamine and related alkaloids in wild plants and tissue cultures of Narcissus confusus by high performance liquid chromatography. Analusis 25: 156-158.
24. Tanahashi T, Poulev A, Zenk MH. 1990. Radiomimunoassay for the quantitative determination of galanthamine. Planta Med. 56: 77-81.
25. Tencheva J, Yamboliev I, Zhivkova Z. 1987. Reversed-phase liquid chromatography for the determination of galanthamine and its metabolites in human plasma and urine. J Chromatogr 421: 396-400.
26. Zhang J, Wang M, Shen Y, Ma G, Hong S. 1999. Studies on alkaloids of amaryllidaceae XII. Identification of amaryllidaceae alkaloids by TLC and determination of galanthamine by HPLC. Yaowu Fenxi Zazhi 19: 399-403.