Low-temperature H2S removal from gas streams with SBA-15 supported ZnO nanoparticles

Chemical Engineering Journal

Volumn 142, Issue 1, 2008, Pages 48-55

  Wang, Xiaohui ^a   Sun, Tonghua ^a   Yang, Ji ^a   Zhao, Ling ^a   Jia, Jinping ^a  

^a SHANGHAI JIAO TONG UNIVERSITY   (China)

Author keywords

Hydrogen sulfide; Mesoporous material; Nanoparticle; Removal

Indexed keywords

ADSORPTION; FOURIER TRANSFORM INFRARED SPECTROSCOPY; GAS ADSORPTION; NITROGEN; OXIDES; SEMICONDUCTING ZINC COMPOUNDS; SILICA; SILICATE MINERALS; SILICON COMPOUNDS; X RAY DIFFRACTION ANALYSIS; ZINC; ZINC OXIDE; ZINC SULFIDE;

IN SITU ACTIVATION; INCIPIENT WETNESS IMPREGNATION; MESOPOROUS; MESOPOROUS SILICA (MPS); NITROGEN ADSORPTION; ULTRASONIC METHODS;

MESOPOROUS MATERIALS;

EID: 47649095742     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2007.11.013     Document Type: Article

References (40)

1. Manahan S.E. Environmental Chemistry. 7th ed. (1997), CRC Press, Boca Raton, FL
2. In: Capone M., Kroschwitz J.K., and Howe-Grant M. (Eds). Encyclopedia of Chemical Technology vol. 23 (1997), Wiley, New York 432
3. Berkow R.Ed. The Merck Manual of Diagnosis and Therapy. 16th ed. (1992), Merck Research Laboratories, Rahway, NJ p. 2691
4. ter Maat H., Hogendoorn J.A., and Versteeg G.F. The removal of hydrogen sulfide from gas streams using an aqueous metal sulfate absorbent. Part II. The regeneration of copper sulfide to copper oxide-an experimental study. Sep. Purif. Technol. 43 (2005) 199-213
5. Stirling D. The Sulfur Problem: Cleaning up Industrial Feedstocks (2000), The Royal Society of Chemistry
6. 2S emission control. Proc. Natl. Acad. Sci. U.S.A. 100 11 (2003) 6308-6312
7. 2 onto oxidized and heat-treated activated carbon fibers (ACFs). Carbon 35 (1997) 411-417
8. Bagreev A., Katikaneni S., Parab S., and Bandosz T.J. Desulfurization of digester gas: prediction of activated carbon bed performance at low concentrations of hydrogen sulfide. Catal. Today 99 (2005) 329-337
9. Thanh D.N., Block K., and Bandosz T.J. Adsorption of hydrogen sulfide on montmorillonites modified with iron. Chemosphere 59 (2005) 343-353
10. Bae M.N., Song M.K., Kim Y., and Seff K. The catalytic activity of vanadium pentoxide film modified electrode on the electrochemical oxidation of hydrogen sulfide in alkaline solutions. Micropor. Mesopor. Mater. 63 (2003) 21-31
11. Khudaish E.A., and Ashraf T.A. The catalytic activity of vanadium pentoxide film modified electrode on the electrochemical oxidation of hydrogen sulfide in alkaline solutions. Electroanal. Chem. 587 (2006) 108-114
12. Nhut J.-M., Vieira R., Pesant L., Tessonnier J.-P., Keller N., Ehret G., Cuong P.-H., and Ledoux M.J. Synthesis and catalytic uses of carbon and silicon carbide nanostructures. Catal. Today 76 (2002) 11-32
13. Schwartz J.A., Contescu C., and Contescu A. Introduction: heterogeneous catalysis. Chem. Rev. 95 3 (1995) 475-476
14. Venuto P.B. Organic catalysis over zeolites: a perspective on reaction paths within micropores. Micropor. Mater. 2 (1994) 297-411
15. Davis M.E., Saldarriaga C., Montes C., Garces J., and Crowder C. A molecular sieve with eighteen-membered rings. Nature 331 (1988) 698-699
16. Schmidt I., Boisen A., Gustavsson E., Stahl K., Pehrson S., Dahl S., Carlsson A., and Jacobsen C.J.H. Carbon nanotube templated growth of mesoporous zeolite single crystals. Chem. Mater. 13 (2001) 4416-4418
17. Kresge C.T., Leonowicz M.E., Roth W.J., Vartuli J.C., and Beck J.S. Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism. Nature 359 (1992) 710-712
18. Zhao D.Y., Feng J.L., Huo Q., Melosh N., Fredrickson G.H., Chmelka B.F., and Stucky G.D. Triblock copolymer syntheses of mesoporous silica with periodic 50-300 Angstrom pores. Science 279 (1998) 548-552
19. Kruk M., Jaroniec M., Kim T.-W., and Ryoo R. Synthesis and characterization of hexagonally ordered carbon nanopipes. Chem. Mater. 15 (2003) 2815-2823
20. 3 and CuO particles and mesostructured SBA-15 silica as an active catalyst for wet peroxide oxidation processes. Catal. Commun. 7 (2006) 478-483
21. Steijns M., Koopman P., Nieuwenhuijse B., and Mars P. The mechanism of the catalytic oxidation of hydrogen sulfide. III. An electron spin resonance study of the sulfur catalyzed oxidation of hydrogen sulfide. J. Catal. 42 (1976) 96-106
22. 2S removal by activated carbons. J. Colloid Interf. Sci. 216 (1999) 360-369
23. Barret E.P., Joyner L.G., and Halenda P.H. The determination of pore volume and area distributions in porous substances. I. Computations from nitrogen isotherms. J. Am. Chem. Soc. 73 (1951) 373-380
24. Ravikovitch P.I., and Neimark A.V. Characterization of micro- and mesoporosity in SBA-15 materials from adsorption data by the NLDFT method. J. Phys. Chem. B 105 (2001) 6817-6823
25. Sing K.S.W., Everett D.H., Haul R.A.W., Moscow L., Pierotti R.A., Rouquerol J., and Siemieniewska T. Reporting physisorption data for gas/solid systems. Pure Appl. Chem. 57 (1985) 603-620
26. Gregg S.J., and Sing K.S.W. Adsorption, Surface Area, and Porosity (1982), Academic Press, London
27. Zhao D.Y., Huo Q.S., Feng J.L., Chmelka B.F., and Stucky G.D. Nonionic triblock and star diblock copolymer and oligomeric surfactant syntheses of highly ordered, hydrothermally stable, mesoporous silica structures. J. Am. Chem. Soc. 120 (1998) 6024-6036
28. Janssen A.H., Yang C.M., Wang Y., Schueth F., Koster A.J., and Jong K.P.D. Localization of small metal (oxide) particles in SBA-15 using bright-field electron tomography. J. Phys. Chem. B 107 (2003) 10552-10556
29. Auroux A., Gervasini A., and Guimon C. Acidic character of metal-loaded amorphous and crystalline silica-aluminas determined by XPS and adsorption calorimetry. J. Phys. Chem. B 103 (1999) 7195-7205
30. Lapkin A., Bozkaya B., Mays T., Borello L., Edler K., and Crittenden B. Preparation and characterization of chemisorbents based on heteropolyacids supported on synthetic mesoporous carbons and silica. Catal. Today 81 (2003) 611-621
31. Günzler H., and Gremlich H.-U. IR Spectroscopy (2002), Wiley-VCH, Weinheim, Germany
32. K.D.O. Jackson, A Guide to Identifying Common Inorganic Fillers and Activators Using Vibrational Spectroscopy, 3rd ed., vol. 2, The Internet Journal of Vibrational Spectroscopy, 1998.
33. Zhang X. Synthesis of 13X molecular sieve from potassium feldspar (in Chinese). China Univ. Geosci. 22 (2003) 167-172
34. Sun Q., Weng S.F., and Zhang X. FTIR microanalysis limits of hydrocarbon fluid inclusions: matrix minerals absorption. Earth Sci.-J. China Univ. Geosci. 23 (1998) 248-252
35. Gaarenstroom S.W., and Winograd N. J. Chem. Phys. 67 (1977) 3500
36. Dake L.S., Baer D.R., and Zachara J.M. Surf. Interf. Anal. 14 (1989) 71
37. Strohmeier B.R., and Hercules D.M. J. Catal. 86 (1984) 266
38. Davidson J.M., Lawrie C.H., and Sohail K. Kinetics of the absorption of hydrogen sulfide by high purity and doped high surface area zinc oxide. Ind. Eng. Chem. Res. 34 (1995) 2981-2989
39. Ahmed M.A., Garcia E., Alonso L., and Palacios J.M. A MS, SEM-EDX and XRD study of Ti or Cu-doped zinc ferrites as regenerable sorbents for hot coal gas desulfurization. Appl. Surf. Sci. 156 (2000) 115-124
40. Christoforou S.C., Efthimiadis E.A., and Vasalos I.A. Sulfidation of mixed metal oxides in a fluidized-bed reactor. Ind. Eng. Chem. Res. 34 (1995) 83-93