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27
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47049099982
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36] (500 mg, 0.16 mmol) was quickly added in small portions with stirring, and at this time, the pH value was 1.74, stirred at room temperature for 1 h, then solid chloride potassium (1 g) was added, and traces of a precipitate were removed by filtration. After slow evaporation in a refrigerator for 18 h, colorless crystals of 1 for X-ray analysis were obtained (yield, 55%). Elemental analysis: Found: K, 5.10; Ti, 3.02; Ge, 2.30; W, 59.38. Calc.
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68: K, 5.06; Ti, 3.11; Ge, 2.36; W, 59.75%.
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28
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33646901345
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Nsouli N.H., Bassil B.S., Dickman M.H., Kortz U., Keita B., and Nadjo L. Inorg. Chem. 45 (2006) 3858
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29
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47049101005
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2 = 0.1215. CSD reference number is 417296.
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2 = 0.1215. CSD reference number is 417296.
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30
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0000255462
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Yamase T., Ozeki T., Sakamoto H., Nishiya S., and Yamamoto A. Bull. Chem. Soc. Jpn. 66 (1993) 103
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Yamase, T.1
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Nishiya, S.4
Yamamoto, A.5
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