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Data for 1. 1H NMR (δ ppm, CDCl3, 0.65 (m, 2H, CH2, 1.21 (t, 9H, CH3, J, 7, 1.64 (m, 2H, CH2, 2.41 (s, 3H, CH3, 2.65 (m, 2H, CH2, 3.79 (q, 6H, CH2, J, 7, 3.89 (s, 2H, CH2, 7.13 (d, 1H, CH, J, 6, 7.26 (d, 1H, CH, J, 6, 8.22 (s, 1H, CH, 8.31 (s, 1H, CH, 8.53 (d, 1H, CH, J, 6, 8.61 (d, 1H, CH, J, 6, 13C {1H) NMR (δ ppm, CDCl3, 7.9 (1C, CH2, 18.3 (3C, CH 3, 21.2 (1C, CH3, 23.4 (1C, CH2, 52.3 (1C, CH2, 53.4 (1C, CH2, 58.2 (3C, CH2, 120.4 (1C, CH, 122.0 (1C, CH, 124.1 (1C, CH, 125.1 (1C, CH, 148.1 (1C, C, 149.0 (1C, CH, 149.2 (1C, CH, 150.8 (1C, C, 156.0, 156.3 (2C, C, 29Si NMR (δ ppm, CDCl3, 45.3 (s, IR(pure, cm-1, 3308 v(NH, 2928 vasCH3,CH2, 2884 v s
-
+.
-
-
-
-
28
-
-
46949087075
-
-
Data for 2. 1H NMR (δ ppm, CDCl3, 0.01 (m, 6H, CH3, 0.51 (m, 2H, CH2, 1.08 (t, 3H, CH 3, J, 6, 1.44 (m, 2H, CH2, 2.36 (s, 3H, CH 3, 2.55 (m, 2H, CH2, 3.55 (q, 2H, CH2, J, 6, 3.78 (s, 2H, CH2, 7.04 (d, 1H, CH, J, 6, 7.22 (d, 1H, CH, J, 6, 8.14 (s, 1H, CH, 8.22 (s, 1H, CH, 8.45 (d, 1H, CH, J, 6, 8.52 (d, 1H, CH, J, 6).13C{1H} NMR (δ ppm, CDCl3, 0.3 (2C, CH3, 13.8 (1C, CH2, 18.5 (1C, CH3, 23.5 (1C, CH3, 23.8 (1C, CH2, 51.8 (1C, CH2, 52.6 (1C, CH2, 58.2 (1C, CH2, 120.9 (1C, CH, 122.0 (1C, CH, 122.9 (1C, CH, 124.9 (1C, CH, 148.1 (1C, C, 148.9 (1C, CH, 149.4 (1C, CH, 150.7 (1C, C, 155.9, 156.3 (2C, C, 29Si NMR (δ ppm, CDCl3, 7.6 (s, IR (pure, cm-1, 3306 vNH, 2960 v as
-
+.
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30
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0000646285
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