Mixing effects in silver halide precipitation: Linking theory with practice using a multi-mechanism model

Chemical Engineering Research and Design

Volumn 82, Issue 9 SPEC. ISS., 2004, Pages 1117-1136

  Kresta, S M ^a   Anthieren, G L ^a   Parsiegla, K ^b  

^a UNIVERSITY OF ALBERTA   (Canada)

^b EASTMAN KODAK COMPANY   (United States)

Author keywords

Lagrangian model; Mixing; Multiscale model; Precipitation; Silver halide

Indexed keywords

COMPUTER SIMULATION; CRYSTALS; DISSOLUTION; IMPELLERS; LAGRANGE MULTIPLIERS; MIXING; NUCLEATION; PRECIPITATION (CHEMICAL); STOICHIOMETRY;

MOLAR FEED RATES; SILVER HALIDE; SIZE-DEPENDENT GROWTH; THERMODYNAMIC EQUILIBRIA;

SILVER COMPOUNDS;

LIQUID-LIQUID MIXING; MODELING; PRECIPITATION; SILVER;

EID: 4644241979     PISSN: 02638762     EISSN: None     Source Type: Journal    
DOI: 10.1205/cerd.82.9.1117.44162     Document Type: Article

References (41)

1. Anthieren, G.L., 2003, Eulerian-lagrangian model of turbulent mixing for silver halide precipitation. Master of Science Thesis, Department of Chemical and Materials Engineering, University of Alberta, Alberta.
2. Antoniades, M.G. and Wey, J.S., 1998, Aggregation phenomena in AgX precipitation in the presence of gelatin, J Imag Sci Technol, 42: 393-398.
3. Baldyga, J. and Bourne, J.R., 1989, Simplification of micromixing calculations. I. Derivation and application of new model, Chem Eng Sci, 42: 83-92.
4. Baldyga, J. and Bourne, J.R., 1999, Turbulent Mixing and Chemical Reactions. (J Wiley, Chichester, UK).
5. Baldyga, J. and Pohorecki, R., 1995, Turbulent mixing in chemical reactors - A review, Chem Eng J, 58: 183-195.
6. Baldyga, J. and Rohani, S., 1987, Micromixing described in terms of inertial-convective disintegration of large eddies and viscous-convective interactions between small eddies, Chem Eng Sci, 42: 2611-2619.
7. Baldyga, J., Bourne, J.R. and Yang Yang, 1993, Influence of feed pipe diameter on mesomixing in stirred tank reactors, Chem Eng Sci, 48: 3383-3390.
8. Baldyga, J., Podgorska, W. and Pohorecki, R., 1995, Mixing precipitation model with application to double feed semibatch precipitation, Chem Eng Sci, 50: 1281-1300.
9. Baldyga, J., Bourne, J.R. and Hearn, S.J., 1997, Interactions between chemical reactions and mixing on various scales, Chem Eng Sci, 52: 457-466.
10. Berry, C.R., 1976, New model for double-jet precipitations, Photogr Sci Eng, 20: 1-4.
11. Berry, C.R. and Skilman, D.C., 1968, Fundamental mechanisms in silver halide precipitation, J Photogr Sci, 16: 137-147.
12. Bourne, J.R. and Yu, S., 1994, Investigation of micromixing in stirred tank reactors using parallel reactions, Ind Eng Chem Res, 33: 41-55.
13. Corrsin, S., 1964, The isotropic turbulent mixer: Part II. Arbitrary Schmidt number, AIChE J, 10: 870-877.
14. David, R., Villermaux, J., Marchal, P. and Klein, J.P., 1991, Crystallization and precipitation engineering IV: kinetic model of adipic acid crystallization, Chem Eng Sci, 46: 1129-1139.
15. Harding, M.J., 1979, The application of calculations of complex solubility to the interpretation of crystal growth phenomena in silver halide emulsions, J Photogr Sci, 27: 1-12.
16. Hounslow, M.J., Ryall, R.L. and Marshall, V.R., 1988, A discretized population balance for nucleation, growth and aggregation, ALChE J, 34: 1821-1832.
17. Jagannathan, R. and Wey, J.S., 1985, Nucleation behavior in the precipitation of a sparingly soluble salt - AgBr, J Cryst Growth, 73: 226-232.
18. James, T.H., 1977, The Theory of the Photographic Process, 4th edn. (Collier Macmillan, London, UK).
19. Jaworski, Z. and Nienow, A.W., 2003, CFD modelling of continuous precipitation of barium sulphate in a stirred tank, Chem Eng J, 91: 167-174.
20. Jézéquel, P.H., 2001, The Concept of 'scaleable reactor' in the precipitation of silver halide photographic microcrystals, Chem Eng Sci, 56: 2399-2408.
21. Johnson, B.K., 2003, Flash nanoprecipitation of organic actives via confined micromixing and block copolymer stabilization, Dissertation, Princeton University.
22. Kharitanova, A.I., Shapiro, B.I. and Bogomolov, K.S., 1979, Z Nauchn Prikl Fotogr Kinematogr, 24: 34.
23. Klein, E. and Moisar, E., 1963, Ber. Bunsenges. Phys. Chem., 67: 349.
24. Kresta, S.M. and Wood, P.E., 1991, Prediction of the three dimensional turbulent flow in stirred tanks, AIChE J, 37: 448-460.
25. Kresta, S.M., Bittorf, K.J. and Wilson, D.J., 2001, Internal annular wall jets: radial flow in a stirred tank, AIChE J, 47: 2390-2401.
26. Leubner, I.H., 1993, Number and size of AgBr crystals as a function of addition rate: a theoretical and experimental review, J Imag Sci, 37: 268-271.
27. Leubner, I.H., 2001, A balanced nucleation and growth model for controlled precipitations, J Dispers Sci Technol, 22: 125-138.
28. Leubner, I.H., Jagannathan, R. and Wey, J.S., 1990, Formation of silver bromide crystals in double-jet precipitation, Photogr Sci Eng, 24: 268-272.
29. Marchal, P., David, R., Klein, J.P. and Villermaux, J., 1988, Crystallization and precipitation engineering I: an efficient method for solving population balance in crystallization with agglomeration, Chem Eng Sci, 43: 59-67.
30. Margolis, G. and Gutoff, E.B., 1974, Simulation of the precipitation of silver bromide photographic emulsions, AIChE J, 20: 467-474.
31. Muhr, H., David, R., Villermaux, J. and Jezequel, P.H., 1995, Crystallization and precipitation engineering V: simulation of the precipitation of silver bromide octahedral crystals in a double-jet semi-batch reactor, Chem Eng Sci, 50: 345-355.
32. Muhr, H., David, R. and Villermaux, J., 1996, Crystallization and precipitation engineering IV: solving population balance in the case of the precipitation of silver bromide crystals with high primary nucleation rates by using first order upwind differentiation, Chem Eng Sci, 51: 309-319.
33. Ostwald, W., 1900, Über die vermeintliche Isomeric des roten und gelben Quecksilberoxyds und die Oberfläschen spannung fester Körper, Z Physik Chem, 22: 289-330.
34. Phillips, R., Rohani, S. and Baldyga, J., 1999, Micromixing in a single feed semi-batch precipitation process, AIChE J, 45: 82-92.
35. Sugimoto, T., 1990, Proceedings 11th Symposium On Industrial Crystallization (Garmisch-Partenkirchen, Germany).
36. Wey, J.S., 1981, Precipitation and Properties of Solid State Materials, Wilcox, W.R. (ed.) Vol. 6, Chap. 2 (Marcel Dekker, New York, USA).
37. Wey, J.S. and Strong, R.W., 1977a, Growth mechanisms of AgBr crystals in gelatin solution, Photogr Sci Eng, 21: 14-18.
38. Wey, J.S. and Strong, R.W., 1977b, Influence of the Gibbs - Thompson effect on the growth behavior of AgBr crystals, Photogr Sci Eng, 21: 248-252.
39. Zauner, R. and Jones, A.G., 2002, On the influence of mixing on crystal precipitation processes - application of the segregated feed model, Chem Eng Sci, 57: 821-831.
40. Zhou, G., and Kresta, S.M., 1996a, Distribution of energy between convective and turbulent flow for three frequently used impellers, Chem Eng Res Des, 74A:379-389.
41. Zhou, G. and Kresta, S.M., 1996b, Impact of geometry on the maximum turbulence energy dissipation rate for various impellers, AIChE J, 42: 2476-2490.