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CCDC-229256 (3) and -229255 (3′) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge at www.ccdc.cam.ac.uk/conts/retrieving.html [or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; Fax: (internat.) + 44-1223-336-033; E-mail: deposit@ccdc.cam.ac.uk].
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brochure from the series "Reagenzien", Merck, Darmstadt
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Trocknen im Labor, brochure from the series "Reagenzien", Merck, Darmstadt.
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