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The mass spectrometer was a high-resolution hybrid double quadrupole (Qq) and orthogonal time-of-flight (TOF) mass spectrometer (QTOF, Micromass UK). The temperature of the nebulizer was 50 °C. The ESI source and the mass spectrometer were operated in the positive-ion mode. The cone and extractor potentials were set to 40-45 and 5-10 V, respectively. The scan range was m/z 50-1000.
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