First acetylenic derivatives of stable 3-imidazoline nitroxides

Tetrahedron Letters

Volumn 45, Issue 41, 2004, Pages 7741-7743

  Vasilevsky, Sergei F ^a   Klyatskaya, Svetlana V ^a   Korovnikova, Olga L ^a   Stass, Dmitri V ^a   Amitina, Svetlana A ^b   Grigir'Ev, Igor A ^b,c   Elguero, José ^d  

^a INSTITUTE OF CHEMICAL KINETICS AND COMBUSTION   (Russian Federation)

^b N N VOROZHTSOV NOVOSIBIRSK INSTITUTE OF ORGANIC CHEMISTRY   (Russian Federation)

^c NOVOSIBIRSK STATE UNIVERSITY   (Russian Federation)

^d INSTITUTO DE QUÍMICA MÉDICA   (Spain)

Author keywords

Imidazoline; Nitroxides; Radicals; Stephens Castro reaction

Indexed keywords

2,2,5,5 TETRAMETHYL 4 [2 (4 IODOPHENYL)VINYL]IMIDAZOLINE 3 OXIDE 1 OL; ACETYLENE DERIVATIVE; ALKYNE DERIVATIVE; COPPER DERIVATIVE; IMIDAZOLINE DERIVATIVE; METHYL GROUP; NITROXIDE DERIVATIVE; PHENYL GROUP; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; SODIUM CHLORIDE; UNCLASSIFIED DRUG;

ARTICLE; CATALYSIS; CHEMICAL REACTION; MOLECULE; RADIOLYSIS; SYNTHESIS;

EID: 4544272191     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2004.08.063     Document Type: Article

References (12)

1. F.B. Sviridenko, D.V. Stass, T.V. Kobzeva, E.V. Tretyakov, S.V. Klyatskaya, E.V. Mshvidobadze, S.F. Vasilevsky, and Y.N. Molin J. Am. Chem. Soc. 126 2004 2807
2. A. Caneschi, D. Gatteschi, and P. Rey Prog. Inorg. Chem. 39 1991 331
3. L.B. Voldarsky, V.A. Reznikov, and V.I. Ovcharenko Synthetic Chemistry of Stable Nitroxides 1994 CRC Boca Raton p 221
4. O. Kahn Molecular Magnetism 1993 VCH New York
5. L.B. Volodarsky Imidazoline Nitroxides 1988 CRC Boca Raton, Florida Synthesis and Properties, Vol. 1, 222 pp and Applications, Vol. 2, 160 pp
6. S.F. Vasilevsky, E.V. Tretyakov, O.M. Usov, Yu.N. Molin, S.V. Fokin, Yu.G. Shwedenkov, V.N. Ikorskii, G.V. Romanenko, R.Z. Sagdeev, and V.I. Ovcharenko Mendeleev Commun. 6 1998 216
7. E.V. Tretyakov, R.I. Samoilova, Yu.V. Ivanov, V.F. Plyusnin, S.V. Pashchenko, and S.F. Vasilevsky Mendeleev Commun. 3 1999 92
8. E.V. Tretyakov, T.V. Novikova, V.V. Korolev, O.M. Usov, S.F. Vasilevsky, and Yu.N. Molin Russ. Chem. Bull. Int. Ed. 49 2000 1409
9. E.V. Tretyakov, D.W. Knight, and S.F. Vasilevsky J. Chem. Soc., Perkin Trans. 1 1999 3713
10. S.F. Vasilevsky, E.V. Tretyakov, and J. Elguero Adv. Heterocycl. Chem. 82 2002 1
11. 13C) = 5.93
12. 3 (aq) and then the organic phase was dried over sodium sulfate, filtered and evaporated to dryness under reduced pressure. Purification of the resulting residue by column chromatography on silica gel (elution with chloroform) followed by crystallization gave the corresponding compounds 2a-f