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13C resonances (unique assignment of the pyrrolide and N-methylpyrrole units and no conformational information was obtained). Full details of the NMR analyses will be published separately.
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14
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85163225702
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note
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3, Z = 6, R = 0.042 for 41973 [I > 2σ(I)) data and wR = 0.049 for 65461 all data. CCDC 219394-219396 (4-6) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223-336033; or deposit@ccdc.cam.ac.uk).
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