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note
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-1): 3665.79(s), 3292(s), 1656.65(s), 1643.75(s), 1633.66(s), 1596.28(s), 1569.29(m), 1557.49(m), 1404.43(w), 936.55(vs), 882.98(vs), 762.13(vs), 669.19(m), 418.42(m).
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44749090003
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note
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2 were 0.0748 and 0.1889, respectively and S = 1.068. X-ray diffraction data were collected on a SMART CCD diffractometer with graphite monochromated Mo Kα radiation at room temperature. The structure was solved by Direct Methods and refined by full-matrix least-squares on F2 with the SHELXL-97 program package.
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