Nonaqueous capillary electrophoresis-electrospray ionization-ion trap-mass spectrometry analysis of pyrrolo- and pyrido[1,2-a]azepine alkaloids in Stemona

Electrophoresis

Volumn 29, Issue 10, 2008, Pages 2079-2087

  Sturm, Sonja ^a   Schinnerl, Johann ^b   Greger, Harald ^b   Stuppner, Hermann ^a  

^a UNIVERSITY OF INNSBRUCK   (Austria)

^b UNIVERSITY OF VIENNA   (Austria)

Author keywords

Nonaqueous capillary electrophoresis electrospray ionization ion trap mass spectrometry; Pyrrolo 1,2 a azepine alkaloids, pyrido 1,2 a azepine alkaloids; Stemonal; Tandem mass spectrometry

Indexed keywords

CAPILLARY ELECTROPHORESIS; ELECTROLYTES; ELECTROSPRAY IONIZATION; MASS SPECTROMETRY; METABOLITES;

AZEPINES; ELECTROSPRAY IONIZATION ION TRAP MASS SPECTROMETRY; NON-AQUEOUS CAPILLARY ELECTROPHORESIS; NONAQUEOUS CAPILLARY ELECTROPHORESIS-ELECTROSPRAY IONIZATION-ION TRAP-MASS SPECTROMETRY; PYRROLO[1,2-A]AZEPINE ALKALOID, PYRIDO[1,2-A] AZEPINE ALKALOID; STEMONA ALKALOIDS; STEMONAL; TANDEM MASS SPECTROMETRY; TANDEM-MASS SPECTROMETRY;

ALKALOIDS;

AZEPINE DERIVATIVE; PLANT EXTRACT; PYRIDO[1,2 A]AZEPINE; PYRROLO[1,2 A]AZEPINE; STEMONA EXTRACT; UNCLASSIFIED DRUG;

ARTICLE; DRUG ANALYSIS; DRUG DETERMINATION; DRUG IDENTIFICATION; ELECTROSPRAY MASS SPECTROMETRY; FRAGMENTATION REACTION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION TRAP MASS SPECTROMETRY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MEASUREMENT ACCURACY; NONAQUEOUS CAPILLARY ELECTROPHORESIS; NONHUMAN; PHYSICAL CHEMISTRY; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; STEMONA; STEMONA CURTISII; STEMONA TUBEROSA; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS;

EID: 44649117560     PISSN: 01730835     EISSN: 15222683     Source Type: Journal    
DOI: 10.1002/elps.200700860     Document Type: Article

References (23)

1. Duyfjes, B. E. E., Stemonaceae, Flora Malesiana ser.l 1993, 11, 399.
2. Pilli, R. A., Rosso, G. B, Ferreira de Oliveira, M. C., Alkaloids Chem. Biol. 2005, 62, 77-173.
3. Greger, H., Planta Med. 2006, 72, 99-113.
4. Stöger, E. A., Arzneibuch der Chinesischen Medizin, Deutscher Apothekerverlag, Stuttgart 1999.
5. Jiang, R.-W., Hon, P.-M., Zhou, Y., Chan, Y.-M. et al., J. Nat. Prod. 2006, 69, 749-754.
6. Zhou, Y., Jiang, R.-W., Hon, P.-M., Xu, Y.-T. et al., Rapid Commun. Mass Spectrom. 2006, 20, 1030-1038.
7. Ye, Y., Lin, L., Tang, C., Lin, G., Velten, R., Planta Med. 2007, 73, issue 09.
8. Lin, L.-G., Zhong, Q.-X., Cheng, T.-Y., Tang, C.-P. et al., J. Nat. Prod. 2006, 69, 1051-1054.
9. Schinnerl, J., Brem, B., But, P. P-H., Vajrodaya, S. et al., Phytochemistry 2007, 68, 1417-1427.
10. Pyne, S. G., Ung, A. T., Jatisatienr, A., Mungkornasawakul, P., Maejo Int. J. Sci. Technol. 2007, 01, 157-165.
11. Brem, B., Seger, C., Pacher, T., Hofer, O. et al., J. Agric. Food. Chem. 2002, 50, 6383-6388.
12. Shinozaki, H., Ishida, M, Brain Res. 1985, 334, 33-40.
13. Chung, H.-S., Hon, P.-M., Lin, G., Nut, P. P.-H., Dong, H., Planta Med. 2003, 69, 914-920.
14. Yang, X.-Z., Tang, C.-P., Ke, C.-Q., Ye, Y., J. Asian Nat. Prod. Res. 2007, 9, 261-266.
15. Pacher, T., Seger, C., Engelmeier, D., Vajrodaya, S. et al., J. Nat. Prod. 2002, 65, 820-927.
16. Kostecki, K., Engelmeier, D., Pacher, T., Hofer, O. et al., Phytochemistry 2004, 65, 99-106.
17. Adams, M., Pacher, T., Greger, H., Bauer, R., J. Nat. Prod. 2005, 68, 83-85.
18. Li, S.-L., Jiang, R.-W., Hon, P-M., Cheng, L. et al., Biomed. Chromatogr. 2007, 21, 1088-1094.
19. Riekkola, M. L., Electrophoresis 2002, 23, 3865-3883.
20. Scriba, G. K. E., J. Chromatogr. A 2007, 1159, 28-41.
21. Sturm, S., Strasser, E. M., Stuppner, H., J. Chromatogr. A 2006, 1112, 331-338.
22. Sturm, S., Seger, C., Stuppner, H., J. Chromatogr. A 2007, 1159, 42-50.
23. Analytical Methods Committee, Analyst 1987, 112, 199.