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2O and 8 ml of water with constant stirring. The homogeneous mixture thus obtained was then dried at 80°C for 5 h. Dried powder was further subjected to calcination in air at 560°C for 12 h. The resultant material showed no structural damage and 1.6% Sn content.
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4444235699
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note
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1H NMR agrees with the structures.
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4444311218
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Melting point matches with the authentic 2g prepared from p-chlorobenzoic acid and hydroquinone.
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37
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