SCOPUS 정보 검색 플랫폼

Volumn 47, Issue 9, 2008, Pages 3492-3494

Mixed-valent dodecanuclear vanadium cluster encapsulating chloride anions and its reaction to form a "bowl"-shaped cluster

(2) Konar, Sanjit a Clearfield, Abraham a

a TEXAS A AND M UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 44149089295 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic800013f Document Type: Article

Times cited : (48)

References (33)

1
- 33751153883
- For examples, see
- (a) For examples, see: Pope, M. T.; Müller, A. Angew. Chem., Int. Ed. Engl. 1991, 30, 34.
- (1991) Angew. Chem., Int. Ed. Engl , vol.30 , pp. 34
- Pope, M.T.¹ Müller, A.²

2
- 0031852282
- (b) Müller, A.; Meyer, J.; Bogge, H.; Stammler, A.; Botar, A. Chem. - Eur. J. 1998, 4, 1388.
- (1998) Chem. - Eur. J , vol.4 , pp. 1388
- Müller, A.¹ Meyer, J.² Bogge, H.³ Stammler, A.⁴ Botar, A.⁵

3
- 0032270594
- (c) Livage, J. Coord. Chem. Rev. 1998, 178, 999.
- (1998) Coord. Chem. Rev , vol.178 , pp. 999
- Livage, J.¹

4
- 0035925753
- (d) Fujita, M.; Umemoto, K.; Yoshizawa, M.; Fujita, N.; Kusukawa, T.; Biradha, K. Chem. Commun. 2001, 509.
- (2001) Chem. Commun , pp. 509
- Fujita, M.¹ Umemoto, K.² Yoshizawa, M.³ Fujita, N.⁴ Kusukawa, T.⁵ Biradha, K.⁶

5
- 0038128307
- (e) Yaghi, O. M.; O'Keeffe, M.; Ockwig, N. W.; Chae, H. K.; Eddaoudi, M.; Kim, J. Nature 2003, 143, 705.
- (2003) Nature , vol.143 , pp. 705
- Yaghi, O.M.¹ O'Keeffe, M.² Ockwig, N.W.³ Chae, H.K.⁴ Eddaoudi, M.⁵ Kim, J.⁶

6
- 44149090373
- (f) Khanra, S.; Kloth, M.; Mansaray, H.; Muryn, C. A.; Tuna, F.; Sanudo, E. C.; Helliwell, M.; McInnes, E. J. L.; Winpenny, R. E. P. Angew. Chem., Int. Ed. 2007, 46, 1.
- (2007) Angew. Chem., Int. Ed , vol.46 , pp. 1
- Khanra, S.¹ Kloth, M.² Mansaray, H.³ Muryn, C.A.⁴ Tuna, F.⁵ Sanudo, E.C.⁶ Helliwell, M.⁷ McInnes, E.J.L.⁸ Winpenny, R.E.P.⁹

7
- 0038413962
- (a) Cotton, F. A.; Donahue, J. P.; Murillo, C. A. J. Am. Chem. Soc. 2003, 125, 5436.
- (2003) J. Am. Chem. Soc , vol.125 , pp. 5436
- Cotton, F.A.¹ Donahue, J.P.² Murillo, C.A.³

8
- 33748219779
- (b) Müller, A.; Hovemeier, K.; Rohlfing, R. Angew. Chem., Int. Ed. Engl. 1992, 31, 1192.
- (1992) Angew. Chem., Int. Ed. Engl , vol.31 , pp. 1192
- Müller, A.¹ Hovemeier, K.² Rohlfing, R.³

9
- 33748237670
- (c) Reuter, H. Angew. Chem., Int. Ed. Engl. 1992, 31, 1185.
- (1992) Angew. Chem., Int. Ed. Engl , vol.31 , pp. 1185
- Reuter, H.¹

10
- 0023859781
- (a) Centi, G.; Trifiro, F.; Ebner, J. R.; Franchetti, V. M. Chem. Rev. 1988, 88, 55.
- (1988) Chem. Rev , vol.88 , pp. 55
- Centi, G.¹ Trifiro, F.² Ebner, J.R.³ Franchetti, V.M.⁴

11
- 2642651895
- (b) Weihe, H.; Güdel, H. U. J. Am. Chem. Soc. 1998, 120, 2870.
- (1998) J. Am. Chem. Soc , vol.120 , pp. 2870
- Weihe, H.¹ Güdel, H.U.²

12
- 0542428069
- (a) Clearfield, A. Chem. Rev. 1988, 88, 125.
- (1988) Chem. Rev , vol.88 , pp. 125
- Clearfield, A.¹

13
- 0034709878
- (b) Do, J.; Bontchev, R. P.; Jacobsen, A. J. Inorg. Chem. 2000, 39, 3230.
- (2000) Inorg. Chem , vol.39 , pp. 3230
- Do, J.¹ Bontchev, R.P.² Jacobsen, A.J.³

14
- 26444590941
- (c) Daniel, C.; Hartl, H. J. Am. Chem. Soc. 2005, 127, 13987.
- (2005) J. Am. Chem. Soc , vol.127 , pp. 13987
- Daniel, C.¹ Hartl, H.²

15
- 0001480202
- (d) Chen, Q.; Zubieta, J. Coord. Chem. Rev. 1992, 114, 107.
- (1992) Coord. Chem. Rev , vol.114 , pp. 107
- Chen, Q.¹ Zubieta, J.²

16
- 2742579772
- (e) Khan, M. I.; Zubieta, J. Prog. Inorg. Chem. 1995, 43.
- (1995) Prog. Inorg. Chem , pp. 43
- Khan, M.I.¹ Zubieta, J.²

17
- 0000205546
- (f) Müller, A.; Peters, F.; Pope, M. T.; Gatteschi, D. Chem. Rev. 1998, 98, 239.
- (1998) Chem. Rev , vol.98 , pp. 239
- Müller, A.¹ Peters, F.² Pope, M.T.³ Gatteschi, D.⁴

18
- 0026381807
- (g) Gatteschi, D.; Pardi, L.; Barra, A.-L.; Müller, A.; Doring, J. Nature 1991, 354, 463.
- (1991) Nature , vol.354 , pp. 463
- Gatteschi, D.¹ Pardi, L.² Barra, A.-L.³ Müller, A.⁴ Doring, J.⁵

19
- 4544316691
- (h) Hegetschweiler, K.; Morgenstern, B.; Zubieta, J.; Hagrman, P. J.; Lima, N.; Sessoli, R.; Totti, F. Angew. Chem., Int. Ed. 2004, 43, 3436.
- (2004) Angew. Chem., Int. Ed , vol.43 , pp. 3436
- Hegetschweiler, K.¹ Morgenstern, B.² Zubieta, J.³ Hagrman, P.J.⁴ Lima, N.⁵ Sessoli, R.⁶ Totti, F.⁷

20
- 0344844576
- and references cited therein
- (a) Müller, A.; Roy, S. Coord. Chem. Rev. 2003, 245, 153. and references cited therein.
- (2003) Coord. Chem. Rev , vol.245 , pp. 153
- Müller, A.¹ Roy, S.²

21
- 0038263047
- 2nd ed, Woollins, J. D, Ed, Wiley-VCH: Weinheim, Germany
- (b) Cronin, L.; Diemann, E.; Müller, A. In Inorganic Experiments, 2nd ed.; Woollins, J. D., Ed.; Wiley-VCH: Weinheim, Germany, 2003; p 340.
- (2003) Inorganic Experiments , pp. 340
- Cronin, L.¹ Diemann, E.² Müller, A.³

22
- 4544354382
- (c) Müller, A.; Das, S. K.; Krickemeyer, E.; Kuhlmann, C. Inorg. Synth. 2004, 34, 191.
- (2004) Inorg. Synth , vol.34 , pp. 191
- Müller, A.¹ Das, S.K.² Krickemeyer, E.³ Kuhlmann, C.⁴

23
- 21244480820
- Rao, C. N. R, Müller, A, Cheetham, A. K, Eds, Wiley-VCH: Weinheim, Germany
- (d) Müller, A.; Roy, S. In The Chemistry of Nanomaterials: Synthesis, Properties and Applications; Rao, C. N. R., Müller, A., Cheetham, A. K., Eds.; Wiley-VCH: Weinheim, Germany, 2004; p 452.
- (2004) The Chemistry of Nanomaterials: Synthesis, Properties and Applications , pp. 452
- Müller, A.¹ Roy, S.²

24
- 0001480202
- (a) Chen, Q.; Zubieta, J. Coord. Chem. Rev. 1992, 114, 107.
- (1992) Coord. Chem. Rev , vol.114 , pp. 107
- Chen, Q.¹ Zubieta, J.²

25
- 2742579772
- and references cited therein
- (b) Khan, M. I.; Zubieta, J. Prog. Inorg. Chem. 1995, 43. and references cited therein.
- (1995) Prog. Inorg. Chem , pp. 43
- Khan, M.I.¹ Zubieta, J.²

26
- 34548155941
- (a) Perry, J. J.; Kravtsov, V. Ch.; McManus, G. J.; Zaworotko, M. J. J. Am. Chem. Soc. 2007, 129, 10076.
- (2007) J. Am. Chem. Soc , vol.129 , pp. 10076
- Perry, J.J.¹ Kravtsov, V.C.² McManus, G.J.³ Zaworotko, M.J.⁴

27
- 0141447391
- (b) Anantharaman, G.; Walawalkar, M. G.; Murugavel Gabor, B.; Herbst-Irmer, R.; Baldus, M.; Angerstein, B.; Roesky, H. W. Angew. Chem., Int. Ed. 2003, 42, 4482.
- (2003) Angew. Chem., Int. Ed , vol.42 , pp. 4482
- Anantharaman, G.¹ Walawalkar, M.G.² Murugavel Gabor, B.³ Herbst-Irmer, R.⁴ Baldus, M.⁵ Angerstein, B.⁶ Roesky, H.W.⁷

28
- 44149105726
- 1H NMR and electrospray ionization mass spectra. Final yield: 2.1 g, 90%.
- 1H NMR and electrospray ionization mass spectra. Final yield: 2.1 g, 90%.

29
- 44149104675
- Synthesis of 1: Anhydrous VCl3 (0.126 g, 0.8 mmol) was taken with biphenylmethylphosphonic acid (0.08 g, 0.3 mmol) and NEt 3 (0.05 g, 0.5 mmol) in acetontrile in an Erlenmeyer flask and refluxed at 80°C for 30 min. The resultant clear green solution was filtered, and the filtrate was kept at room temperature. After 2 days, X-ray-quality green single crystals had grown. The initial and final pH values of the reaction were 2.5 and 3.0, respectively. The yield of the reaction was ∼20, on the basis of vanadium, Elem anal. Calcd, C, 43.54; H, 4.60; N, 2.46. Found: C, 44.36; H, 4.12; N, 2.88. Selected IR data (KBr pellet, 3110(s, 2927(m, 2820(m) 1573(w, 1442(w, 1350(w, 1055(s, 787(m, 755(m, 549(m, 506(m) cm-1, b) Synthesis of 2:1 was taken with VCl 3 (1:1) in Py and CH3CN (1:1) in an Erlenmeyer flask and refluxed at 80°C for 4 h. The resultant clear green solution was filtered, and the filtrate was kep
- -1. 2 has also been synthesized following the same procedure as that for 1, except that the same equivalent of pyridine was taken instead of triethylamine. Large orange crystals were grown up from the solution, and an unidentified green oil separated out. The yield of the reaction was ∼20% (on the basis of vanadium).

30
- 44149086725
- Crystallographic data for 1 (at 110 K, M, 3653.37, triclinic, P1, a, 17.528(11) Å, b, 19.255(12) Å, c, 25.444(15) Å, α, 86.430(11)°, β, 81.083(10)°, γ, 78.355(11)°, V, 4641(2) Å3, Z, 2, R1, 0.1453, wR2, 0.4024. The R factor of the compound is very high because of the presence of highly disordered triethylaammonium cations. Crystallographic data for 2: M, 3371.18, hexagonal, P62c, a, 16.8442(16) Å, b, 16.8442(16) Å, c, 34.778(7) Å, α, 90.00°, β, 90.00°, γ, 120.00°, V, 8546(2) Å3, Z, 2, R1, 0.0632, wR2, 0.1809. One phenyl ring of the phosphonate ligand is disordered over two positions and was not assigned to hydrogen atoms. Three atoms of the pyridine near sandwiched chlorides were symmetry-generated from the other three. So, the
- 3, Z = 2, R1 = 0.0632, wR2 = 0.1809. One phenyl ring of the phosphonate ligand is disordered over two positions and was not assigned to hydrogen atoms. Three atoms of the pyridine near sandwiched chlorides were symmetry-generated from the other three. So, the nitrogen atom could not be assigned. This is due to the fact that those pyridines are in different orientations in the packing and the X-ray data gave us an averaged diffraction pattern.

31
- 84922260578
- Breese, N. E.; O'Keefe, M. Acta Crystallogr. 1991, B47, 192.
- (1991) Acta Crystallogr , vol.B47 , pp. 192
- Breese, N.E.¹ O'Keefe, M.²

32
- 33750274533
- (a) Chang, Y. D.; Salta, J.; Zubieta, J. Angew. Chem., Int. Ed. Engl. 1994, 33, 325.
- (1994) Angew. Chem., Int. Ed. Engl , vol.33 , pp. 325
- Chang, Y.D.¹ Salta, J.² Zubieta, J.³

33
- 51149211339
- (b) Chen, Q.; Zubieta, J. Chem. Commun. 1994, 1635.
- (1994) Chem. Commun , pp. 1635
- Chen, Q.¹ Zubieta, J.²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.