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note
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c of the oxygen-rich sample was found to be 70 K, which is lower than that of the pristine sample.
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31
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4344564380
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note
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In the course of thermal analysis, the iodine intercalate was heated from room temperature to 800 °C at a rate of 20 °C/min in a flowing Ar gas. The disintercalated chemical species during thermal analysis were analyzed by using a quadrupole mass spectrometer (electron impacting type E1, VG Scientific). The evolved gas was instantly introduced into the mass spectrometer through a flexible capillary. Energy of the impacting electron used in the mass spectrometer was 70 eV.
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