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43049158247
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note
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3, 20 °C, δ from TMS): 7.49 (s, 8H; Ar), 1.20 ppm (s, 36H; t-Bu).
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29
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43049169056
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note
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int = 0.048), 6035 observed reflections (I > 2.00σ(I)), 536 parameters, R = 0.0562, wR = 0.1636, refined against {divides}F{divides}, GOF = 0.996. Crystallographic data of the crystals have been deposited at the Cambridge Crystallographic Data Center in CIF format CCDC no. 631424. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (e-mail:deposit@ccdc.cam.ac.uk).
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