Isothermal nucleation and growth kinetics of Pd/Ag alloy phase via in situ time-resolved high-temperature X-ray diffraction (HTXRD) analysis

Journal of Membrane Science

Volumn 316, Issue 1-2, 2008, Pages 97-111

  Ayturk, M Engin ^a   Payzant, E A ^b   Speakman, S A ^b   Ma, Y H ^a  

^a Worcester Polytechnic Institute   (United States)

^b OAK RIDGE NATIONAL LABORATORY   (United States)

Author keywords

Composite Pd Ag alloy membranes; Electroless plating; H2 separation; In situ time resolved high temperature X ray diffraction; Isothermal annealing

Indexed keywords

ELECTROLESS PLATING; ISOTHERMAL ANNEALING; NUCLEATION; X RAY DIFFRACTION ANALYSIS;

COMPOSITE PD/AG ALLOY MEMBRANES; HYDROGEN SEPARATION;

PALLADIUM ALLOYS;

PALLADIUM; SILVER;

ELECTROLESS PLATING; ISOTHERMAL ANNEALING; NUCLEATION; PALLADIUM ALLOYS; X RAY DIFFRACTION ANALYSIS;

ARTICLE; COMPUTER PROGRAM; ENERGY EXPENDITURE; HIGH TEMPERATURE; ISOTHERM; KINETICS; PRIORITY JOURNAL; X RAY DIFFRACTION;

EID: 42949099543     PISSN: 03767388     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.memsci.2007.09.038     Document Type: Article

References (51)

1. Uemiya S., Sato N., Ando H., Kude Y., Matsuda T., and Kikuchi E. Separation of hydrogen through palladium thin film supported on a porous glass tube. J. Membr. Sci. 56 3 (1991) 303
2. Shu J., Grandjean B.P.A., Van Neste A., and Kaliaguine S. Catalytic palladium-based membrane reactors; a review. Can. J. Chem. Eng. 69 (1991) 1036-1060
3. Gryaznov V.M., Serebyannikova O.S., and Serov Y.M. Preparation and catalysis over palladium composite membranes. Appl. Catal. A: Gen. 96 (1993) 15-23
4. Mardilovich P.P., She Y., Ma Y.H., and Rei M.-H. Defect-free palladium membranes on porous stainless-steel support. AIChE J. 44 2 (1998) 310
5. Shu J., Grandjean B.P.A., Van Neste A., and Kaliaguine S. Catalytic palladium-based membrane reactors: a review. Can. J. Chem. Eng. 69 (1991) 1036-1060
6. Ma Y.H., Akis B.C., Ayturk M.E., Guazzone F., Engwall E.E., and Mardilovich I.P. Characterization of intermetallic diffusion barrier and alloy formation for Pd/Cu and Pd/Ag porous stainless steel composite membranes. Ind. Eng. Chem. Res. 43 12 (2004) 2936-2945
7. Ayturk M.E., Engwall E.E., and Ma Y.H. XRD phase analysis on the alloying of binary Pd/PSS, Ag/PSS and ternary Pd/Ag/PSS systems. Proceedings of the 2005 North American Membrane Society Annual Meeting (NAMS 2005). Providence, RI, United States (2005)
8. Ayturk M.E., Engwall E.E., and Ma Y.H. Microstructure analysis of the intermetallic diffusion induced alloy phases in composite Pd/Ag/porous stainless steel (PSS) membranes. Ind. Eng. Chem. Res. 46 12 (2007) 4295
9. Ayturk M.E., Mardilovich I.P., Engwall E.E., and Ma Y.H. Synthesis of composite Pd-porous stainless steel (PSS) membranes with a Pd/Ag intermetallic diffusion barrier. J. Membr. Sci. 285 1-2 (2006) 385
10. Uemiya S., Matsuda T., and Kikuchi E. Hydrogen permeable palladium-silver alloy membrane supported on porous ceramics. J. Membr. Sci. 56 3 (1991) 315
11. Shu J., Grandjean B.P.A., Ghali E., and Kaliaguine S. Simultaneous deposition of Pd and Ag on porous stainless steel by electroless plating. J. Membr. Sci. 77 2-3 (1993) 181
12. Cheng Y.S., and Yeung K.L. Palladium-silver composite membranes by electroless plating technique. J. Membr. Sci. 158 1-2 (1999) 127
13. Huang T.-C., Wei M.-C., and Chen H.-I. Preparation of hydrogen-permselective palladium-silver alloy composite membranes by electroless co-deposition. Sep. Purif. Technol. 32 (2003) 239-245
14. Keuler J.N., Lorenzen L., Sanderson R.D., Prozesky V., and Pryzbylowicz W.J. Characterization of electroless plated palladium-silver alloy membranes. Thin Solid Films 347 (1999) 91-98
15. Li A., Liang, Weiqiang, Hughes, and Ronald. Characterization and permeation of palladium/stainless steel composite membranes. J. Membr. Sci. 149 (1998) 259-268
16. Keuler J.N., and Lorenzen L. Developing a heating procedure to optimize hydrogen permeance through Pd-Ag membranes of thickness less than 2.2 μm. J. Membr. Sci. 195 2 (2002) 203
17. Hou K., and Hughes R. Preparation of thin and highly stable Pd/Ag composite membranes and simulative analysis of transfer resistance for hydrogen separation. J. Membr. Sci. 214 (2003) 43-55
18. Shu J., Adnot A., Grandjean B.P.A., and Kaliaguine S. Structurally stable composite Pd-Ag alloy membranes: introduction of a diffusion barrier. Thin Solid Films 286 (1996) 72-79
19. 2 separation. Proceedings of the Eighth International Conference on Inorganic Membranes (ICIM8). Cincinnati, OH, United States (2004)
20. JADE6.5, A Program for Powder Diffraction Data Analysis, Materials Data Inc., Livermore, CA, USA.
21. 2 thin films grown from bilayer InSe/CuSe precursors. J. Vac. Sci. Technol. A 23 2 (2005) 310-315
22. 8 and their dependence on precursor chemistry. J. Mater. Chem. 12 (2002) 990-994
23. Cullity B.D., and Stock S.R. Elements of X-ray Diffraction. 3rd ed. (2001), Prentice Hall, Upper Saddle River, NJ
24. King H.W., Payzant E.A., and Caughlin T.A. Temperature discrepancies in high-temperature diffractometry. Adv. Xray Anal. 40 (1997-1998) 679
25. J.A. Brand, H.J. Goldschmidth, B.S.A. Group Research Center Sheffield, GRC/G 1109, 1955.
26. Touloukian Y.S., Kriby R.K., Taylor R.E., and Desai P.D. Thermal expansion: metallic elements and alloys. Thermophys. Properties Matter 12 (1977) 298
27. Karakaya I., and Thompson W.T. The Pd-Ag system. Bull. Alloy Phase Diagrams 9 3 (1988) 237-243
28. Burke J. The Kinetics of Phase Transformations in Metals (1965), Pergamon Press Ltd., Oxford
29. 2 separation. Proceedings of the International Hydrogen Energy Congress and Exhibition (IHEC 2005). Istanbul, Turkey (2005)
30. Anderson W., and Mehl R. Recrystallization of Al in terms of the rate of nucleation and growth. Trans. AIME 161 (1945) 140
31. Avrami M. Kinetics of phase change. I. General theory. J. Chem. Phys. 7 (1939) 1103-1112
32. Avrami M. Kinetics of phase change. II. Transformation-time relations for random distribution of nuclei. J. Chem. Phys. 8 (1940) 212-224
33. Avrami M. Kinetics of phase change. III. Granulation, phase change on microstructures. J. Chem. Phys. 9 (1941) 177-184
34. Choi S.Y., Mamak M., Speakman S., Chopra N., and Ozin G.A. Evolution of nanocrystallinity in periodic mesoporous anatase thin films. Small 1 2 (2005) 226-232
35. Johnson W., and Mehl R. Reaction kinetics in processes of nucleation and growth. Trans. AIME 135 (1939) 416-458
36. A. Kolmogorov, A statistical theory for the recrystallization of metals, Akad. Nauk. SSSR, Izv., Ser. Matem. 1 (1937) 355.
37. Becker R. Ann. Phys. 32 (1938) 128
38. Becker R. Proc. Phys. Soc. 52 (1940) 71
39. Christian J.W. The Theory of Transformations in Metals and Alloys: An Advanced Textbook in Physical Metallurgy (1965), Pergamon Press
40. Cahn J.W. Acta Metall. 4 (1956) 449
41. Porter D.A., and Easterling K.E. Phase Transformations in Metals and Alloys (1992), CRC Press
42. Magee C.L. Metall. Trans. 2 (1971) 2419
43. Friel J.J. X-ray and Image Analysis in Electron Microscopy (1998), Princeton-Gamma Tech, Princeton, NJ
44. Nachtrieb N.H., Petit J., and Wehrenberg J. Self-diffusion of Ag in silver-palladium alloys. J. Chem. Phys. 26 (1957) 106
45. Rowland R.L., and Nachtrieb N.H. Self-diffusion of palladium in silver-palladium alloys. J. Phys. Chem. 67 (1963) 2817
46. Peterson N.L. Phys. Rev. 132 (1963) 2471
47. Brown A.M., and Ashby M.F. Correlations for diffusion constant. Acta Metall. 28 (1980) 1085
48. Neumann G., and Tolle V. Phil. Mag. A 54 (1986) 619
49. Peterson N.L. Phys. Rev. 136 (1964) 568
50. Crank J. The Mathematics of Diffusion (1975), Oxford University Press, Ely House, London
51. Brandes E.A., and Brook G.B. Smithells Metals Reference Book. 7th ed. (1998), Elsevier