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Crystallographic data. 1: C40H56N 4P2Pt·C7H8, M, 942.05, T, 173(2) K, monoclinic, space group P2 1/c (No. 14, a, 13.3845(2) Å, b, 22.7704(3) Å, c, 15.5458(2) Å, β, 104.780(1)°, U, 4581.13(11) Å3, Z, 4, Dc, 1.37 Mg m-3, μ(Mo Kα, 3.17 mm-1, independent reflections, 7728 [Rint, 0.058, R1 [for 6438 reflections with I > 2σ(I, 0.030, wR2 (all data, 0.063. 2: C40H80N4P2Pt, M, 874.11, T, 173(2) K, monoclinic, space group P2 1/c (No. 14, a, 11.8881(2) Å, b, 17.9465(3) Å, c, 21.0820(3) Å, β, 94.286(1)°, U, 4485.26(12) Å3, Z
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int = 0.087], R1 [for 5932 reflections with I > 2σ(I)] = 0.049, wR2 (all data) = 0.103.
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The P-dicyclohexylphosphaguanidinate anion was shown to bridge between Li atoms via the Nimine atom in the cyclic hexamer [Li(Cy2PC{NiPr}2)]6. See ref 5
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