Synthesis, characterization, and mass-transport properties of two novel gadolinium(III) hexafluoroacetylacetonate polyether adducts: Promising precursors for MOCVD of GdF3 films

Chemistry of Materials

Volumn 8, Issue 6, 1996, Pages 1292-1297

  Malandrino, Graziella ^a   Incontro, Ornella ^a   Castelli, Francesco ^a   Fragalà, Ignazio L ^a   Benelli, Cristiano ^b  

^a UNIVERSITY OF CATANIA   (Italy)

^b UNIVERSITY OF FLORENCE   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

EVAPORATION RATE; FILM DEPOSITION; HIGH VOLATILITY; LIQUID PHASE; MOCVD PRECURSORS; MONONUCLEAR STRUCTURES; SINGLE-CRYSTAL X-RAY DIFFRACTION STUDIES; THERMAL BEHAVIORS;

CRYSTAL STRUCTURE; DEPOSITION; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; THERMOANALYSIS; TRANSPORT PROPERTIES; X RAY DIFFRACTION;

GADOLINIUM;

EID: 4243766003     PISSN: 08974756     EISSN: 15205002     Source Type: Journal    
DOI: 10.1021/cm950569c     Document Type: Article

References (36)

1. Mehrotra, R. C.; Bohra, R.; Gaur, D. P. Metal β-diketonates and Allied Derivatives; Academic Press: London, 1978.
2. Bradley, D. C.; Mehrotra, R. C.; Gaur, D. P. Metal Alkoxides; Academic Press: London, 1978.
3. Sievers, R. E.; Sadlowski, J. E. Science 1978, 201, 217.
4. Mehrotra, R. C.; Singh, A.; Tripathi, U. M. Chem. Rev. 1991, 91, 1287.
5. Yang, K. N.; Dalichaouch, Y.; Ferreira, J. M.; Lee, B. W.; Neumeier, J. J.; Torikachvili, M. S.; Zhou, H.; Maple, M. B.; Hake, R. R. Solid State Commun. 1987, 63, 515.
6. Engler, E. M.; Lee, V. Y.; Nazzal, A. I.; Beyers, R. B.; Lim, G.; Grant, P. M.; Parkin, S. S. P.; Ramirez, M. L.; Vasquez, J. E.; Savoy, R. J. J. Am. Chem. Soc. 1987, 109, 2848.
7. Vaidya, K. J.; Yang, C. Y.; DeGraef, M.; Lange, F. F. J. Mater. Res. 1994, 9, 410.
8. Blasse, G. Chem. Mater. 1994, 6, 1465.
9. (a) Hölsä, J.; Kestilä, E. J. Chem. Soc., Faraday Trans. 1995, 91, 1503.
10. (b) Hölsä, J.; Kestilä, E. J. Alloy Comp. 1995, 225, 89.
11. (a) Chemical Vapor Deposition: Principles and Applications (Hitchman, M. L., Jensen, K. F., Eds.; Academic Press: London, 1993.
12. (b) Spencer, J. T. In Progress in Inorganic Chemistry; (Karlin, K. D., Ed.; John Wiley & Sons Inc.: New York, 1994; Vol. 41, p 145.
13. Sato, H. Jpn. J. Appl. Phys. 1994, 33, L371.
14. Amano, R.; Shiokawa, Y.; Sato, N.; Suzuki, Y. J. Radioanal. Nucl. Chem. 1993, 172, 81.
15. (a) Richardson, M. F.; Wagner, W. F.; Sands, D. E. J. Inorg. Nucl. Chem. 1968, 30, 1275.
16. (b) Richardson, M. F.; Sievers, R. E. Inorg. Chem. 1971, 10, 498.
17. Plakatouras, J. C.; Baxter, I.; Hursthouse, M. B.; Abdul Malik, K. M.; McAleese, J.; Drake, S. R. J. Chem. Soc., Chem. Commun. 1994, 2455.
18. Timmer, K.; Spee, K. I. M. A.; Mackor, A.; Meinema, H. A.; Spek, A. L.; Van der Sluis, P. Inorg. Chim. Acta 1991, 190, 109.
19. Gardiner, R.; Brown, D. W.; Kirlin, P. S.; Rheingold, A. L. Chem. Mater. 1991, 3, 1053.
20. Drake, R. S.; Miller, S. A. S.; Williams, D. J. Inorg. Chem. 1993, 32, 3227.
21. Neumayer, D. A.; Studebaker, D. B.; Hinds, B. J.; Stern, C. L.; Marks, T. J. Chem. Mater. 1994, 6, 878.
22. (a) Malandrino, G.; Fragalà, I. L.; Neumayer, D. A.; Stern, C. L.; Hinds, B. J.; Marks, T. J. J. Mater. Chem. 1994, 4, 1061.
23. (b) Shamlian, S. H.; Hitchman, H. L.; Cook, S. L.; Richards, B. C. J. Mater. Chem. 1994, 4, 81.
24. Malandrino, G.; Castelli, F.; Fragalà, I. L. Inorg. Chim. Acta 1994, 224, 203.
25. Malandrino, G.; Licata, R.; Castelli, F.; Fragalà, I. L.; Benelli, C. Inorg. Chem. 1995, 34, 6233.
26. 160Gd.
27. 2O has been synthesized as reported in ref 13.
28. Malandrino, G.; Fragalà, I. L., unpublished results.
29. (a) Benelli, C.; Caneschi, A.; Gatteschi, D.; Laugier, J.; Rey, P. Angew. Chem., Int. Ed. Engl. 1987, 26, 913.
30. (b) Benelli, C.; Caneschi, A.; Gatteschi, D.; Pardi, L.; Rey, P. Inorg. Chem. 1989, 28, 275.
31. (c) Benelli, C.; Caneschi, A.; Gatteschi, D.; Pardi, L.; Rey, P. Inorg. Chem. 1990, 29, 4223.
32. Baxter, I.; Drake, S. R.; Hursthouse, M. B.; Abdul Malik, K. M.; McAleese, J.; Otway, D. J.; Plakatouras, J. C. Inorg. Chem. 1995, 34, 1384.
33. Richardson, M. F.; Wagner, W. F.; Sands, D. E. Inorg. Chem. 1968, 7, 2495.
34. Drake, S. R.; Lyons, A.; Otway, D. J.; Slawin, A. M. Z.; Williams, D. J. J. Chem. Soc., Dalton Trans. 1993, 2379.
35. Hitchman, M. L.; Shamlian, S. H.; Gilliland, D. C.; Cole-Hamilton, D.; Nash, J. A. P.; Thompson, S. C.; Cook, S. L. J. Mater. Chem. 1995, 5, 47.
36. 2O sample leaves a much greater residue (32%) at 430°C than the fresh material.