메뉴 건너뛰기




Volumn 69, Issue 7, 1996, Pages 216-231

Structural characterization of concentrated alkaline silicate solutions by 29Si-NMR spectroscopy, FT-IR spectroscopy, light scattering, and electron microscopy - Molecules, colloids, and dissolution artefacts

Author keywords

[No Author keywords available]

Indexed keywords


EID: 4243203414     PISSN: 09467475     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article
Times cited : (12)

References (32)
  • 1
  • 2
    • 0002124080 scopus 로고
    • Soluble silicates - Their properties and uses
    • Technology. New York: Reinhold (Am. Chem. Soc. Monograph Series.)
    • Vail, J. G.: Soluble silicates - their properties and uses. Vol. 1. Chemistry. Vol. 2. Technology. New York: Reinhold 1952. (Am. Chem. Soc. Monograph Series.)
    • (1952) Chemistry , vol.1-2
    • Vail, J.G.1
  • 3
    • 0007981164 scopus 로고
    • Soluble silicates
    • Washington, DC: Am. Chem. Soc.
    • Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc. 1982. (Am. Chem. Soc. Symp. Ser. 194.)
    • (1982) Am. Chem. Soc. Symp. Ser. 194
    • Falcone, J.S.1
  • 4
    • 0023953056 scopus 로고
    • Natriumwasserglaslösungen - Aufbau, Eigenschaften und Probleme
    • Hoebbel, D.; Ebert, R.: Natriumwasserglaslösungen - Aufbau, Eigenschaften und Probleme. Z. Chem. 28 (1988) p. 41-51.
    • (1988) Z. Chem. , vol.28 , pp. 41-51
    • Hoebbel, D.1    Ebert, R.2
  • 5
    • 0003149022 scopus 로고
    • Application of silicon-29 and aluminium-27 NMR to determine the distribution of anions in sodium silicate and sodium alumino silicate solutions
    • McCormick, A. V.; Bell, A. T.; Radke, C. J.: Application of silicon-29 and aluminium-27 NMR to determine the distribution of anions in sodium silicate and sodium alumino silicate solutions. Stud. Surf. Sci. Catal. 28 (1986) p. 247-254.
    • (1986) Stud. Surf. Sci. Catal. , vol.28 , pp. 247-254
    • McCormick, A.V.1    Bell, A.T.2    Radke, C.J.3
  • 7
    • 37049078526 scopus 로고
    • 29Si nuclear magnetic resonance linewidths in aqueous silicate aolutions and their effect on exchange rate determination
    • 29Si nuclear magnetic resonance linewidths in aqueous silicate aolutions and their effect on exchange rate determination. J. Chem. Soc., Dalton Trans. (1986) p. 2265-2269.
    • (1986) J. Chem. Soc., Dalton Trans. , pp. 2265-2269
    • Griffiths, L.1    Cundy, C.S.2    Plaisted, R.J.3
  • 8
    • 37049110297 scopus 로고
    • 4- group exchange between silicate anions in aqueous alkaline silicate solutions
    • 4- group exchange between silicate anions in aqueous alkaline silicate solutions. J. Chem. Soc., Chem. Commun. 8 (1984) p. 514-516.
    • (1984) J. Chem. Soc., Chem. Commun. , vol.8 , pp. 514-516
    • Engelhardt, G.1    Hoebbel, D.2
  • 9
    • 0001785505 scopus 로고
    • Silicon-29 NMR studies of aqueous silicate solutions. Pt. 2. Isotopic enrichment
    • Harris, R. K.; Jones, J.; Knight, C. T. G.: Silicon-29 NMR studies of aqueous silicate solutions. Pt. 2. Isotopic enrichment. J. Mol. Struct. 69 (1980) p. 95-103.
    • (1980) J. Mol. Struct. , vol.69 , pp. 95-103
    • Harris, R.K.1    Jones, J.2    Knight, C.T.G.3
  • 10
    • 33845557235 scopus 로고
    • Nature of species present in an aqueous solution of potassium silicate
    • Harris, R. K.; Knight, C. T. G.; Hull, W. E.: Nature of species present in an aqueous solution of potassium silicate. J. Am. Chem. Soc. 103 (1981) p. 1577-1578.
    • (1981) J. Am. Chem. Soc. , vol.103 , pp. 1577-1578
    • Harris, R.K.1    Knight, C.T.G.2    Hull, W.E.3
  • 11
    • 0001792516 scopus 로고
    • Silicon-29 NMR studies of aqueous silicate solutions
    • Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc.
    • Harris, R. K.; Knight, C. T. G.; Hull, W. E.: Silicon-29 NMR studies of aqueous silicate solutions. In: Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc. 1982. p. 79-93. (Am. Chem. Soc. Symp. Ser. 194.)
    • (1982) Am. Chem. Soc. Symp. Ser. 194 , pp. 79-93
    • Harris, R.K.1    Knight, C.T.G.2    Hull, W.E.3
  • 12
    • 4344583072 scopus 로고
    • Silicon-29 nuclear magnetic resonance studies of aqueous silicate solutions. Pt. 5. First-order patterns in potassium silicate solutions enriched with silicon-29
    • Harris, R. K.; Knight, C. T. G.: Silicon-29 nuclear magnetic resonance studies of aqueous silicate solutions. Pt. 5. First-order patterns in potassium silicate solutions enriched with silicon-29. J. Chem. Soc., Faraday Trans. II 79 (1983) p. 1525-1538.
    • (1983) J. Chem. Soc., Faraday Trans. II , vol.79 , pp. 1525-1538
    • Harris, R.K.1    Knight, C.T.G.2
  • 13
    • 4344593977 scopus 로고
    • Silicon-29 nuclear magnetic resonance studies of aqueous silicate solutions. Pt. 6. Second-order patterns in potassium silicate solutions enriched with silicon-29
    • Harris, R. K.; Knight, C. T. G.: Silicon-29 nuclear magnetic resonance studies of aqueous silicate solutions. Pt. 6. Second-order patterns in potassium silicate solutions enriched with silicon-29. J. Chem. Soc., Faraday Trans. II 79 (1983) p. 1539-1561.
    • (1983) J. Chem. Soc., Faraday Trans. II , vol.79 , pp. 1539-1561
    • Harris, R.K.1    Knight, C.T.G.2
  • 14
    • 0040777973 scopus 로고
    • Two-dimensional silicon-29 NMR studies of aqueous silicate solutions
    • Harris, R. K.; O'Connor, M. J.; Curzon, E. H. et al.: Two-dimensional silicon-29 NMR studies of aqueous silicate solutions. J. Magn. Resonance 57 (1984) p. 115-122.
    • (1984) J. Magn. Resonance , vol.57 , pp. 115-122
    • Harris, R.K.1    O'Connor, M.J.2    Curzon, E.H.3
  • 15
    • 84989069040 scopus 로고
    • Quantitative silicon-29 NMR investigations of highly concentrated high-ratio sodium silicate solutions
    • Harris, R.K.; Bahlmann, E. K. F.; Metcalfe, K. et al.: Quantitative silicon-29 NMR investigations of highly concentrated high-ratio sodium silicate solutions. Magn. Resonance Chem. 3 (1993) p. 743-747.
    • (1993) Magn. Resonance Chem. , vol.3 , pp. 743-747
    • Harris, R.K.1    Bahlmann, E.K.F.2    Metcalfe, K.3
  • 16
    • 79957548994 scopus 로고
    • Silicon NMR studies on dissolved silicates
    • Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc.
    • Marsmann, H. C.; Vongehr , M.: Silicon NMR studies on dissolved silicates. In: Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc. 1982. p. 73-78. (Am. Chem. Soc. Symp. Ser. 194.)
    • (1982) Am. Chem. Soc. Symp. Ser. 194 , pp. 73-78
    • Marsmann, H.C.1    Vongehr, M.2
  • 17
    • 0022289444 scopus 로고
    • Herstellung, Struktur und Chemie technisch wichtiger Alkalisilicate
    • Christophliemk, P.: Herstellung, Struktur und Chemie technisch wichtiger Alkalisilicate. Glastech. Ber. 58 (1985) no. 11, p. 308-314.
    • (1985) Glastech. Ber. , vol.58 , Issue.11 , pp. 308-314
    • Christophliemk, P.1
  • 18
    • 0000082891 scopus 로고
    • Silicate minerals as sources of trimethylsilyl silicates and silicate structure analysis of sodium silicate solutions
    • Lentz, C. W.: Silicate minerals as sources of trimethylsilyl silicates and silicate structure analysis of sodium silicate solutions. Inorg. Chem. 3 (1969) p. 574-579.
    • (1969) Inorg. Chem. , vol.3 , pp. 574-579
    • Lentz, C.W.1
  • 19
    • 0011239011 scopus 로고
    • Studies on sodium silicate solutions by the method of trimethylsilylation
    • Dent Glasser, L. S.; Lachowski, E. E.; Cameron, G. G.: Studies on sodium silicate solutions by the method of trimethylsilylation. J. Appl. Chem. Biotechnol. 27 (1977) p. 39-47.
    • (1977) J. Appl. Chem. Biotechnol. , vol.27 , pp. 39-47
    • Dent Glasser, L.S.1    Lachowski, E.E.2    Cameron, G.G.3
  • 20
    • 0002896799 scopus 로고
    • Polymerization and colloid formation in silicate solutions
    • Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc.
    • Andersson, K. R.; Dent Glasser, L. S.; Smith, D. N.: Polymerization and colloid formation in silicate solutions. In: Falcone, J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc. 1982. p. 115-131. (Am. Chem. Soc. Symp. Ser. 194.)
    • (1982) Am. Chem. Soc. Symp. Ser. 194 , pp. 115-131
    • Andersson, K.R.1    Dent Glasser, L.S.2    Smith, D.N.3
  • 21
  • 22
    • 4243080507 scopus 로고
    • Colloidal components in solutions of sodium silicate
    • Falcone , J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc.
    • Her, R. K.: Colloidal components in solutions of sodium silicate . In.: Falcone , J. S. (ed.): Soluble silicates. Washington, DC: Am. Chem. Soc. 1982. p. 95-113. (Am. Chem. Soc. Symp. Ser. 194.)
    • (1982) Am. Chem. Soc. Symp. Ser. 194 , pp. 95-113
    • Her, R.K.1
  • 23
    • 4243108014 scopus 로고
    • A Raman and infrared study of aqueous solutions of sodium silicates as a function of pH
    • Marinangeli, A.; Morell, M. A.; Simoni, R. et al.: A Raman and infrared study of aqueous solutions of sodium silicates as a function of pH. Can. J. Spectrosc. 23 (1978) p. 173-177.
    • (1978) Can. J. Spectrosc. , vol.23 , pp. 173-177
    • Marinangeli, A.1    Morell, M.A.2    Simoni, R.3
  • 24
    • 4243146898 scopus 로고
    • Uber die Anwendung der Farbstoffadsorptionsmethode zur Charakterisierung von Natriumsilicat(Wasserglas)-Lösungen
    • Hoebbel, D.; Ebert, R.; Wieker, W. et al.: Uber die Anwendung der Farbstoffadsorptionsmethode zur Charakterisierung von Natriumsilicat(Wasserglas)-Lösungen. Z. anorg. allg. Chem. 558 (1988) p. 171-188.
    • (1988) Z. Anorg. Allg. Chem. , vol.558 , pp. 171-188
    • Hoebbel, D.1    Ebert, R.2    Wieker, W.3
  • 25
    • 4243073783 scopus 로고
    • Differences in molecular species present in aqueous potassium silicate solutions and their efficiency as adhesives for phosphors on glass
    • Walker, A. J.; Whitehead, N.: Differences in molecular species present in aqueous potassium silicate solutions and their efficiency as adhesives for phosphors on glass. J. Appl. Chem. 16 (1966) p. 230-238.
    • (1966) J. Appl. Chem. , vol.16 , pp. 230-238
    • Walker, A.J.1    Whitehead, N.2
  • 27
    • 36849125881 scopus 로고
    • Raman spectral studies of water structure
    • Walrafen, G. E.: Raman spectral studies of water structure. J. Chem. Phys. 40 (1964) p. 3249-3256.
    • (1964) J. Chem. Phys. , vol.40 , pp. 3249-3256
    • Walrafen, G.E.1
  • 28
    • 0002736906 scopus 로고
    • Der Einbau des Wassers in Gläsern. II. UR-Messungen an Silikatgläsern mit systematisch variierter Zusammensetzang und Deutung der OH-Banden in Silikatgläsern
    • Scholze, H.: Der Einbau des Wassers in Gläsern. II. UR-Messungen an Silikatgläsern mit systematisch variierter Zusammensetzang und Deutung der OH-Banden in Silikatgläsern. Glastech. Ber. 32 (1959) no. 4, p. 142-152.
    • (1959) Glastech. Ber. , vol.32 , Issue.4 , pp. 142-152
    • Scholze, H.1
  • 29
    • 0000830842 scopus 로고
    • The Raman and the IR spectrum of the aqueous silicate ion
    • Fortnum, D.; Edwards, J. O.: The Raman and the IR spectrum of the aqueous silicate ion. J. Inorg. Nucl. Chem. 2 (1956) p. 264-265.
    • (1956) J. Inorg. Nucl. Chem. , vol.2 , pp. 264-265
    • Fortnum, D.1    Edwards, J.O.2
  • 30
    • 0024139282 scopus 로고
    • Thermodynamic stability of monodispersed particles in solution
    • Strehlow, P.: Thermodynamic stability of monodispersed particles in solution. J. Non-Cryst. Solids 107 (1988/89) p. 55-60.
    • (1988) J. Non-Cryst. Solids , vol.107 , pp. 55-60
    • Strehlow, P.1
  • 32
    • 0011444983 scopus 로고
    • Silicate glasses
    • Lutze, W; Ewing, R. C. (eds.): Amsterdam (et al.): North-Holland
    • Lutze, W: Silicate glasses. In: Lutze, W; Ewing, R. C. (eds.): Radioactive waste forms for the future. Amsterdam (et al.): North-Holland 1988. p. 1-159.
    • (1988) Radioactive Waste Forms for the Future , pp. 1-159
    • Lutze, W.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.