Synthesis, characterization, and molecular structure of bis{(tert-butyldimethylsilyl)-tetramethylcyclopentadienyl}lead

Organometallics

Volumn 15, Issue 19, 1996, Pages 3905-3906

  Constantine, Steven P ^a   Hitchcock, Peter B ^a   Lawless, Gerard A ^a  

^a UNIVERSITY OF SUSSEX   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 4243097378     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om960511n     Document Type: Article

References (13)

1. Constantine, S. P.; Hitchcock, P. B.; Lawless, G. A.; De Lima, G. M. J. Chem. Soc., Chem. Commun. 1996, 1101-1102.
2. Bombieri, G.; Panattoni, C. Acta Crystallogr. 1966, 20, 595.
3. Panattoni, C.; Bombieri, G.; Croatto, U. Acta Crystallogr. 1966, 21, 823-826.
4. Atwood, J. L.; Hunter, W. E.; Cowley, A. H.; Jones, R. A.; Stewart, C. A. J. Chem. Soc., Chem. Commun. 1981, 925-927.
5. Schumann, H.; Janiak, C.; Hahn, E.; Kolax, C.; Loebel, J.; Rausch, M. D.; Zuckerman, J. J.; Heeg, M. J. Chem. Ber. 1986, 119, 2656-2667.
6. Heeg, M. J.; Janiak, C.; Zuckerman, J. J. J. Am. Chem. Soc. 1984, 106, 4259-4261.
7. Heeg, M. J.; Herber, R. H.; Janiak, C.; Zuckerman, J. J.; Schumann, H.; Manders, W. F. J. Organomet. Chem. 1988, 346, 321-332.
8. 2Pb: C, 52.66 (53.14); H. 8.04 (8.03).
9. 2) = 0.104 for all 3903 reflections.
10. 207Pb. respectively. At spin rates in excess of 8 kHz a variable-amplitude (triangular ramp ± 30%) cross-polarization contact pulse was employed. The principal components of the chemical shift tensors have been determined from spinning sideband analysis.
11. Keates, J. M.; Lawless, G. A. Manuscript in preparation.
12. Janiak, C.; Schumann, H.; Stader, C.; Wrackmeyer, B.; Zuckerman, J. J. Chem. Ber. 1988, 121, 1745-1751.
13. Wrackmeyer, B.; Stader, C.; Horchler, K. J. Mag. Reson. 1989, 83, 601-607.