Morphology and amine accessibility of (3-aminopropyl) triethoxysilane films on glass surfaces

Scanning

Volumn 30, Issue 2, 2008, Pages 65-77

  Wang, Wei ^a   Vaughn, Mark W ^a  

^a Department of Electrical and Computer Engineering   (United States)

Author keywords

APTES; Atomic force microscopy; Bioconjugation; Fluorescence microscopy; Image analysis; Optical imaging; Silanol

Indexed keywords

AMINES; ANNEALING; ATOMIC FORCE MICROSCOPY; CHEMICAL VAPOR DEPOSITION; GLASS; SURFACE MORPHOLOGY;

BIOCONJUGATION; OPTICAL IMAGING; PICRIC ACID; SILANOL;

THIN FILMS;

AMINE; GLASS; PICRIC ACID; RHODAMINE; SILANE DERIVATIVE;

ARTICLE; ATOMIC FORCE MICROSCOPY; CHEMICAL REACTION; CONJUGATION; FLUORESCENCE MICROSCOPE; METHODOLOGY; OPTICS; PRIORITY JOURNAL; TEMPERATURE;

AMINES; COATED MATERIALS, BIOCOMPATIBLE; FLUORESCENCE; GLASS; MICROSCOPY, ATOMIC FORCE; SILANES;

EID: 42349083304     PISSN: 01610457     EISSN: None     Source Type: Journal    
DOI: 10.1002/sca.20097     Document Type: Article

References (74)

1. Allen G, Sorbello F, Altavilla C, Castorina A, Ciliberto E: Macro-, micro- and nano-investigations on 3-aminopropyl trimethoxysilane self-assembly-monolayers. Thin Solid Films 483, 306-311 (2005).
2. Banks PR, Paquette DM: Comparison of 3 common amine reactive fluorescent-probes used for conjugation to biomolecules by capillary zone electrophoresis. Bioconjug Chem 6, 447-458 (1995).
3. Bekiari V, Lianos P: Characterization of photoluminescence from a material made by interaction of (3-aminopropyl)triethoxysilane with acetic acid. Langmuir 14, 3459-3461 (1998).
4. Benitez JJ, Ogletree DF, Salmeron M: Preparation and characterization of self-assembled multilayers of octadecylamine on mica from ethanol solutions. Langmuir 19, 3276-3281 (2003).
5. Born M, Wolf E: Principles of Optics, Cambridge University Press, Cambridge (1980).
6. Chechik V, Stirling CJM: Reactivity in self-assembled monolayers, effect of the distance from the reaction center to the monolayer-solution interface. Langmuir 14, 99-105 (1998).
7. Chen QZ, Rezwan K, Armitage D, Nazhat SN, Boccaccini AR: The surface functionalization of 45s5 bioglass (r)-based glass-ceramic scaffolds and its impact on bioactivity. J Mater Sci Mater Med 17, 979-987 (2006).
8. Crampton N, Bonass WA, Kirkham J, Thomson NH: Formation of aminosilane-functionalized mica for atomic force microscopy imaging of DNA. Langmuir 21, 7884-7891 (2005).
9. Crampton N, Bonass WA, Kirkham J, Thomson NH: Studying silane mobility on hydrated mica using ambient AFM. Ultramicroscopy 106, 765-770 (2006).
10. Drexhage KH: Influence of a dielectric interface on fluorescence decay time. J Luminescence 1-2, 693 (1970).
11. Ek S, Iiskola EI, Niinisto L: Gas-phase deposition of aminopropylalkoxysilanes on porous silica. Langmuir 19, 3461-3471 (2003).
12. 2/Si surface. Langmuir 23, 6119-6125 (2007).
13. Etienne M, Walcarius A: Analytical investigation of the chemical reactivity and stability of aminopropyl-grafted silica in aqueous medium. Talanta 59, 1173-1188 (2003).
14. Falsey JR, Renil M, Park S, Li SJ, Lam KS: Peptide and small molecule microarray for high throughput cell adhesion and functional assays. Bioconjug Chem 12, 346-353 (2001).
15. Fan FQ, Maldarelli C, Couzis A: Fabrication of surfaces with nanoislands of chemical functionality by the phase separation of self-assembling monolayers on silicon. Langmuir 19, 3254-3265 (2003).
16. Foisner J, Glaser A, Kattner J, Hoffmann H, Friedbacher G: Atomic force microscopy investigation of the growth of different alkylsiloxane monolayers from highly concentrated solutions. Langmuir 19, 3741-3746 (2003).
17. Frey A, Neutra MR, Robey FA: Peptomer aluminum oxide nanoparticle conjugates as systemic and mucosal vaccine candidates: synthesis and characterization of a conjugate derived from the C4 domain of HIV-1 (MN) gp120. Bioconjug Chem 8, 424-433 (1997).
18. Garcia-Turiel J, Jerome B: Solvent retention in thin polymer films studied by gas chromatography. Colloid Polym Sci 285, 1617-1623 (2007).
19. Gaur RK, Gupta KC: A spectrophotometric method for the estimation of amino-groups on polymer supports. Anal Biochem 180, 253-258 (1989).
20. Gisin BF: The monitoring of reactions in solid-phase peptide synthesis with picric acid. Anal Chim Acta 58, 248-249 (1972).
21. Gyorvary E, Wetzer B, Sleytr UB, Sinner A, Offenhausser A, et al.: Lateral diffusion of lipids in silane-, dextran-, and s-layer-supported mono- and bilayers. Langmuir 15, 1337-1347 (1999).
22. Heiney P, Gruneberg K, Fang J, Dulcey C, Shashidhar R: Structure and growth of chromophore-functionalized (3-aminopropyl)triethoxysilane self-assembled on silicon. Langmuir 16, 2651-2657 (2000).
23. Hermanson GT: Bioconjugate Techniques, Academic Press, New York (1999).
24. Howarter JA, Youngblood JP: Optimization of silica silanization by 3-aminopropyl triethoxysilane. Langmuir 22, 11142-11147 (2006).
25. Howarter JA, Youngblood JP: Surface modification of polymers with 3-aminopropy ltriethoxysilane as a general pretreatment for controlled wettability. Macromolecules 40, 1128-1132 (2007).
26. Hu J, Wang M, Weier HUG, Frantz P, Kolbe W, et al.: Imaging of single extended DNA molecules on flat (aminopropyl)triethoxysilane-mica by atomic force microscopy. Langmuir 12, 1697-1700 (1996).
27. Jin L, Horgan A, Levicky R: Preparation of end-tethered DNA monolayers on siliceous surfaces using heterobifunctional cross-linkers. Langmuir 19, 6968-6975 (2003).
28. Joos B, Kuster H, Cone R: Covalent attachment of hybridizable oligonucleotides to glass supports. Anal Biochem 247, 96-101 (1997).
29. Jung GY, Li ZY, Wu W, Chen Y, Olynick DL, et al.: Vapor-phase self-assembled monolayer for improved mold release in nanoimprint lithography. Langmuir 21, 1158-1161 (2005).
30. Kanan SA, Tze WTY, Tripp CP: Method to double the surface concentration and control the orientation of adsorbed (3-aminopropyl)dimethylethoxysilane on silica powders and glass slides. Langmuir 18, 6623-6627 (2002).
31. Kang HJ, Blum FD: Structure and dynamics of amino functional silanes adorbed on silica surfaces. J Phys Chem 95, 9391-9396 (1991).
32. Keller H: Objective lenses for confocal microscopy. In Handbook of Biological Confocal Microscopy, (Ed. Pawley J), Springer Science+Business, New York, 145-161 (2006).
33. Kessel CR, Granick S: Formation and characterization of a highly ordered and well-anchored alkylsilane monolayer on mica by self-assembly. Langmuir 7, 532-538 (1991).
34. Kim SR, Abbott NL: Manipulation of the orientational response of liquid crystals to proteins specifically bound to covalently immobilized and mechanically sheared films of functionalized bovine serum albumin. Langmuir 18, 5269-5276 (2002).
35. Koga T, Morita M, Ishida H, Yakabe H, Sasaki S, et al.: Dependence of the molecular aggregation state of octadecylsiloxane monolayers on preparation methods. Langmuir 21, 905-910 (2005).
36. Kurth DG, Bein T: Surface reactions on thin layers of silane coupling agents. Langmuir 9, 2965-2973 (1993).
37. Kurth DG, Bein T: Thin-films of (3-aminopropyl)triethoxysilane on aluminum-oxide and gold substrates. Langmuir 11, 3061-3067 (1995).
38. Legrange JD, Markham JL, Kurkjian CR: Effects of surface hydration on the deposition of silane monolayers on silica. Langmuir 9, 1749-1753 (1993).
39. LeProust E, Zhang H, Yu PL, Zhou XC, Gao XL: Characterization of oligodeoxyribonucleotide synthesis on glass plates. Nucleic Acids Res 29, 2171-2180 (2001).
40. Macdonald RI: Characteristics of self-quenching of the fluorescence of lipid-conjugated rhodamine in membranes. J Biol Chem 265, 13533-13539 (1990).
41. Martin HJ, Schulz KH, Bumgardner JD, Walters KB: XPS study on the use of 3-aminopropyltriethoxysilane to bond chitosan to a titanium surface. Langmuir 23, 6645-6651 (2007).
42. Matsumoto A, Tsutsumi K, Schumacher K, Unger KK: Surface functionalization and stabilization of mesoporous silica spheres by silanization and their adsorption characteristics. Langmuir 18, 4014-4019 (2002).
43. McGovern ME, Kallury KMR, Thompson M: Role of solvent on the silanization of glass with octadecyltrichlorosilane. Langmuir 10, 3607-3614 (1994).
44. Metwalli E, Haines D, Becker O, Conzone S, Pantano C: Surface characterizations of mono-, di-, and tri-aminosilane treated glass substrates. J Colloid Interface Sci 298, 825-831 (2006).
45. Miyazaki M, Kaneno J, Uehara M, Fujii M, Shimizu H, et al.: Simple method for preparation of nanostructure on microchannel surface and its usage for enzyme-immobilization. Chem Commun, (5), 648-649 (2003).
46. Moon JH, Shin JW, Kim SY, Park JW: Formation of uniform aminosilane thin layers: an imine formation to measure relative surface density of the amine group. Langmuir 12, 4621-4624 (1996).
47. Moon JH, Kim JH, Kim K, Kang TH, Kim B, et al.: Absolute surface density of the amine group of the aminosilylated thin layers: ultraviolet-visible spectroscopy, second harmonic generation, and synchrotron-radiation photoelectron spectroscopy study. Langmuir 13, 4305-4310 (1997).
48. Nakagawa T, Ogawa K, Kurumizawa T: Atomic-force microscope images of monolayers from alkyltrichlorosilane on mica surfaces and studies on an anchoring mechanism of alkyltrichlorosilane molecules to the surface. Langmuir 10, 525-529 (1994).
49. Nashat AH, Moronne M, Ferrari M: Detection of functional groups and antibodies on microfabricated surfaces by confocal microscopy. Biotechnol Bioeng 60, 137-146 (1998).
50. Ngo TT: A simple spectrophotometric determination of solid supported amino-groups. J Biochem Biophys Methods 12, 349-354 (1986).
51. Pantano CG. Surface chemistry in relation to the strength and fracture of silicate glasses. In Strength of Inorganic Glass, (Ed. Kurkjian CR). Plenum Press: New York, 37-66 (1985).
52. Peanasky J, Schneider HM, Granick S, Kessel CR: Self-assembled monolayers on mica for experiments utilizing the surface forces apparatus. Langmuir 11, 953-962 (1995).
53. Peters RD, Nealey PF, Crain JN, Himpsel FJ: A near edge x-ray absorption fine structure spectroscopy investigation of the structure of self-assembled films of octadecyltrichlorosilane. Langmuir 18, 1250-1256 (2002).
54. Rasband WS, Image J. U. S. National Institutes of Health, Bethesda, Maryland, http://rsb.info.nih.gov/ij/, (1997-2007).
55. Richardson H, Sferrazza M, Keddie JL: Influence of the glass transition on solvent loss from spin-cast glassy polymer thin films. Eur Phys J E 12, S87-S91 (2003).
56. Rozlosnik N, Gerstenberg MC, Larsen NB: Effect of solvents and concentration on the formation of a self-assembled monolayer of octadecylsiloxane on silicon (001). Langmuir 19, 1182-1188 (2003).
57. Simon A, Cohen-Bouhacina T, Porte M, Aime J, Baquey C: Study of two grafting methods for obtaining a 3-aminopropyltriethoxysilane monolayer on silica surface. J Colloid Interface Sci 251, 278-283 (2002).
58. Stevens MJ: Thoughts on the structure of alkylsilane monolayers. Langmuir 15, 2773-2778 (1999).
59. Sun CH, Aston DE, Berg JC: Structural evolution of octyltriethoxysilane films on glass surfaces during annealing at elevated temperature. J Colloid Interface Sci 248, 96-102 (2002).
60. Szabo A, Gournis D, Karakassides MA, Petridis D: Clay-aminopropylsiloxane compositions. Chem Mater 10, 639-645 (1998).
61. Tidswell IM, Rabedeau TA, Pershan PS, Kosowsky S, Folkers JP, et al.: X-ray grazing-incidence diffraction from alkylsiloxane monolayers on silicon-wafers. J Chem Phys 95, 2854-2861 (1991).
62. Uchida Y, Nobu YI, Momiji I, Matsui K: Luminescence of silica-pillared clays and gels derived from aminofunctional silanes. J Sol-Gel Sci Technol 19, 705-709 (2000).
63. Ulman A: Formation and structure of self-assembled monolayers. Chem Rev 96, 1533-1554 (1996).
64. Vaidya AA, Norton ML: DNA attachment chemistry at the flexible silicone elastomer surface: toward disposable microarrays. Langmuir 20, 11100-11107 (2004).
65. Vandenberg E, Bertilsson L, Liedberg B, Uvdal K, Erlandsson R, et al.: Structure of 3-aminopropyl triethoxy silane on silicon oxide. J Colloid Interface Sci 147, 103-118 (1991).
66. Waddell TG, Leyden DE, Debello MT: The nature of organosilane to silica-surface bonding. J Am Chem Soc 103, 5303-5307 (1981).
67. 2. Langmuir 19, 1159-1167 (2003).
68. Wang B, Abdulali-Kanji Z, Dodwell E, Horton JH, Oleschuk RD: Surface characterization using chemical force microscopy and the flow performance of modified polydimethylsiloxane for microfluidic device applications. Electrophoresis 24, 1442-1450 (2003).
69. White LD, Tripp CP: Reaction of (3-aminopropyl)dimethylethoxysilane with amine catalysts on silica surfaces. J Colloid Interface Sci 232, 400-407 (2000).
70. Wikstrom P, Mandenius CF, Larsson PO: Gas-phase silylation, a rapid method for preparation of high-performance liquid-chromatography supports. J Chromatogr 455, 105-117 (1988).
71. Xiao XD, Liu GY, Charych DH, Salmeron M: Preparation, structure, and mechanical stability of alkylsilane monolayers on mica. Langmuir 11, 1600-1604 (1995).
72. Yu L, Li CM, Zhou Q, Gan Y, Bao QL: Functionalized multi-walled carbon nanotubes as affinity ligands. Nanotechnology 18, 116614 (2007).
73. Zhang FX, Srinivasan MP: Self-assembled molecular films of aminosilanes and their immobilization capacities. Langmuir 20, 2309-2314 (2004).
74. Zhuang XW, Ha T, Kim HD, Centner T, Labeit S, et al.: Fluorescence quenching: a tool for single-molecule protein-folding study. Proc Natl Acad Sci USA 97, 14241-14244 (2000).