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Crystal data for 11: C36H52O10, M, 644.78, colorless plate, 0.12 x 0.12 x 0.09 mm3, monoclinic, space group P21 No. 4, a, 10.4893(2) Å, b, 7.7835(2) Å, c, 21.1003(5) Å, β, 93.518(1)°, V, 1719.46(7) Å3, Z, 2, Dc, 1.245 g/cm3, F000, 696, Nonius Kappa CCD diffractometer, Mo Kα radiation, λ, 0.71073 Å, T, 113(2) K, 2θmax, 51.3°, 6480 reflections collected, 6480 unique (Rint, 0.0000, Final GooF, 1.049, R1, 0.0573, wR2, 0.1399, R indices based on 5199 reflections with I >2σI refinement on F2, 430 parameters, 1 restraint. Lp corrections applied, μ, 0.090 mm -1. H atoms added in idealized positions in a riding model with isotropic thermal para
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