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Crystallographic data for EuGS-1: crystal of dimensions 0.05 x 0.06 x 0.25 mm, monoclinic, space group I2/a, Mr, 696.98, and a, 22.555(2) Å, b, 7.3428(7) Å, c, 14.929(1) Å, β, 90.137(2)°, V, 2472.4(4) Å3, Z, 8, dcalcd, 3.745 g cm -3, μ(Mo Kα, 15.476 cm-1. A total of 8587 reflections were measured at 294 K, which gave 3067 independent reflections with Rint, 0.0249. R1, 0.0293 and wR2, 0.0786 for 2802 reflections with I > 2σ(I) and 181 parameters. Crystallographic data for the REGS-1 materials are summarized in Table S1, selected bond lengths and bond angles are given in Table S2. The unit cell dimensions for GdGS-1 and TbGS-1 are smaller because of lanthanide contraction
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int = 0.0249. R1 = 0.0293 and wR2 = 0.0786 for 2802 reflections with I > 2σ(I) and 181 parameters. Crystallographic data for the REGS-1 materials are summarized in Table S1, selected bond lengths and bond angles are given in Table S2. The unit cell dimensions for GdGS-1 and TbGS-1 are smaller because of lanthanide contraction.
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