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Volumn 47, Issue 6, 2008, Pages 1901-1903

Synthesis of Ge2NiS4 clusters and the thermal transformation to a Ge4Ni6S12 cluster

Author keywords

[No Author keywords available]

Indexed keywords

GERMANIUM; METALLOPROTEIN; NICKEL; SULFUR;

ARTICLE; CHEMISTRY; THERMODYNAMICS;

GERMANIUM; METALLOPROTEINS; NICKEL; SULFUR; THERMODYNAMICS;

EID: 42149112951 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic702379y Document Type: Article

Times cited : (10)

References (14)

1
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- Steifel, E. I, Matsumoto K, Eds, American Chemical Society: Washington, DC
- (a) Transition Metal Sulfur Chemistry, Biological and Industrial Significance; Steifel, E. I., Matsumoto K., Eds.; American Chemical Society: Washington, DC, 1996.
- (1996) Transition Metal Sulfur Chemistry, Biological and Industrial Significance

2
- 0003666155
- Weber, Th, Prons, R, van Santen, R. A, Eds, Kluwer Academic Publishers: Dordrecht, The Netherlands
- (b) Transition Metal Sulphides - Chemistry and Catalysis; Weber, Th., Prons, R., van Santen, R. A., Eds.; Kluwer Academic Publishers: Dordrecht, The Netherlands, 1998.
- (1998) Transition Metal Sulphides - Chemistry and Catalysis

3
- 0003617813
- Springer-Verlag: Berlin
- (a) Topsøe, H.; Clausen, B. S.; Massoth, F. E. Hydrotreating Catalysis: Science and Technology; Springer-Verlag: Berlin, 1996.
- (1996) Hydrotreating Catalysis: Science and Technology
- Topsøe, H.¹ Clausen, B.S.² Massoth, F.E.³

4
- 0003410045
- Kondasa-Wiley-VCH: Tokyo
- (b) Kabe, T.; Ishihara, A.; Qian, W. Hydrodesulfurization and Hydrodenitrogenation: Chemistry and Engineering; Kondasa-Wiley-VCH: Tokyo, 1999.
- (1999) Hydrodesulfurization and Hydrodenitrogenation: Chemistry and Engineering
- Kabe, T.¹ Ishihara, A.² Qian, W.³

5
- 42149173513
- In press
- (a) Matsumoto, T.; Nakaya, Y.; Itakura, N.; Tatsumi, K. J. Am. Chem. Soc. In press.
- J. Am. Chem. Soc
- Matsumoto, T.¹ Nakaya, Y.² Itakura, N.³ Tatsumi, K.⁴

6
- 42149161431
- In press
- (b) Matsumoto, T.; Nakaya, Y.; Tatsumi, K. Angew. Chem., Int. Ed. In press.
- Angew. Chem., Int. Ed
- Matsumoto, T.¹ Nakaya, Y.² Tatsumi, K.³

7
- 33749842932
- (c) Matsumoto, T.; Nakaya, Y.; Tatsumi, K. Organometallics 2006, 25, 4835.
- (2006) Organometallics , vol.25 , pp. 4835
- Matsumoto, T.¹ Nakaya, Y.² Tatsumi, K.³

8
- 61349109707
- In press
- Matsumoto, T.; Matsui, Y.; Ito, M.; Tatsumi, K. Chem. Asian J. In press.
- Chem. Asian J
- Matsumoto, T.¹ Matsui, Y.² Ito, M.³ Tatsumi, K.⁴

9
- 42149155185
- Crystal data for 2: C74H74Ge 2NiP2S4; monoclinic; C2/c (No. 15, a, 30.814(3) Å b, 21.9372(16) Å c, 30.454(3) Å; β, 127.5838(18)°, V, 16311(3) Å Z, 8; T, 193 K; λ, 0.71073 Å; F(000, 5632; μ, 11.363 cm-1; ρcalcd, 1.105 g cm -3; 91 233 reflections (2θ < 55.0°, 18 666 unique (Rint, 0.093, R1, 0.0860 (I > 2σ(I, wR2, 0.2642 (all data, GOF (on F 2, 1.367. Crystal data for 3·1.5toluene: C 94.5H92Ge2NiP2S4; triclinic; P1 (No. 2, a, 14.0364(14) Å b, 18.010(3) Å c, 18.085(3) Å; α, 106.910(6)°, β, 107.7173(13)°, γ, 95.117(2)°, V, 4086.6(9) A
- 2. Anisotropic refinement was applied to all non-hydrogen atoms. All the hydrogen atoms were put at calculated positions, except for those of the disordered crystalline solvent molecules, two toluenes for 3 and a dichloromethane for 5.

10
- 0004009372
- 6th ed, John Wiley & Sons: New York
- Cotton, F. A.; Wilkinson, G.; Murillo, G. Advanced Inorganic Chemistry, 6th ed.; John Wiley & Sons: New York, 1999; pp 840-842..
- (1999) Advanced Inorganic Chemistry , pp. 840-842
- Cotton, F.A.¹ Wilkinson, G.² Murillo, G.³

11
- 42149192874
- -1. The fraction containing 5 was observed at 45 min retention time, while 1 has a significantly longer 49 min retention time.
- -1. The fraction containing 5 was observed at 45 min retention time, while 1 has a significantly longer 49 min retention time.

12
- 42149193435
- Synthesis of [DmpGe(μ-S)3]4Ni6 (5, A toluene solution of 3 (200 mg, 0.135 mmol) was heated for 12 h at 110°C. The crude product was separated by GPC (CHCl3, 3.5 mL/min) to give a fraction of 45 min retention time, which was further crystallized by EtOH/CH2Cl2 to give 5 (27 mg) as a red crystals. The yield calculated on the basis of nickels is 53, 1H NMR (500 MHz, CDCl3, δ, 7.47 (t, J, 7.6 Hz, 4H, p-CH of Dmp, 6.98 (s, 16H, m-CH of Mes, 6.97 (d, J, 7.6 Hz, 8H, m-CH of Dmp, 2.27 (s, 24H, p-CH3 of Mes, 1.83 (s, 48H, o-CH3 of Mes, Elemental analysis calcd, ) for C96H100Ge4Ni6S12: C, 50.55; H, 4.42; S, 16.87. Found: C, 49.98; H, 4.02; S, 16.90
- 12: C, 50.55; H, 4.42; S, 16.87. Found: C, 49.98; H, 4.02; S, 16.90.

13
- 42149186734
- McCleverty, J. A, Meyer, T. J, Eds, Elsevier: Amsterdam
- Meyer, F.; Kozlowski, H. In Comprehensive Coordination Chemistry II; McCleverty, J. A., Meyer, T. J., Eds.; Elsevier: Amsterdam, 2004; Vol. 6, pp 322-342..
- (2004) Comprehensive Coordination Chemistry II , vol.6 , pp. 322-342
- Meyer, F.¹ Kozlowski, H.²

14
- 0029499890
- Baines, K. M.; Stibbs, W. G. Coord. Chem. Rev. 1995, 145, 157.
- (1995) Coord. Chem. Rev , vol.145 , pp. 157
- Baines, K.M.¹ Stibbs, W.G.²

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