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Angewandte Chemie - International Edition

Volumn 47, Issue 10, 2008, Pages 1958-1960

Syntheses with a chiral building block from the citric acid cycle: (2R,3S)-isocitric acid by fermentation of sunflower oil

(6) Heretsch, Philipp a Thomas, Franziska a Aurich, Andreas b Krautscheid, Harald a Sicker, Dieter a Giannis, Athanassios a

a UNIVERSITY OF LEIPZIG (Germany)

b HELMHOLTZ CENTRE FOR ENVIRONMENTAL RESEARCH UFZ (Germany)

Author keywords

Chiral pool; Citric acid cycle; Green chemistry; Isocitric acid

Indexed keywords

BIOCHEMICAL ENGINEERING; CHEMICAL REACTIONS; CITRIC ACID; FERMENTATION; PRECIPITATION (CHEMICAL); SEPARATION; SYNTHESIS (CHEMICAL); VEGETABLE OILS;

CHIRAL POOL; CITRIC ACID CYCLE; GREEN CHEMISTRY; ISOCITRIC ACID;

ACIDS;

ISOCITRIC ACID; SUNFLOWER OIL; VEGETABLE OIL;

ARTICLE; BIOTECHNOLOGY; CHEMICAL STRUCTURE; CHEMISTRY; CITRIC ACID CYCLE; FERMENTATION; METABOLISM; STEREOISOMERISM; X RAY CRYSTALLOGRAPHY;

BIOTECHNOLOGY; CITRIC ACID CYCLE; CRYSTALLOGRAPHY, X-RAY; FERMENTATION; ISOCITRATES; MODELS, MOLECULAR; MOLECULAR STRUCTURE; PLANT OILS; STEREOISOMERISM;

EID: 41949124708 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200705000 Document Type: Article

Times cited : (42)

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- Crystal data of C16H24O6: Stoe IPDS-2T diffractometer, Mm, 312.35 gmol-1, crystal size 0.1 × 0.4 × 0.9 mm3, monoclinic, space group P21 (no. 4, a, 821.95(9, b, 561.50(4, c, 1760.2(2) pm, β, 97.141(9)°, V, 806.07(14) × 106 pm3, Z, 2, T, 180(2) K, ρcalcd, 1.287 gcm-3, μ, 0.098 mm-1, λ, 71.073 pm (MoKα, 10207 measured, 2805 independent reflections, Rint, 0.073, 2608 with I > 2σ(I, 207 parameters, H atoms in idealized positions, R1 (observed reflections, 0.051, wR2 (all data, 0.15, max/min residual electron density peaks 0.21/-0.20 e × 106 pm3; structure solution and refinement: SHELX-97 G. M. Sheldrick, SHELXS-97, Program
- 3; structure solution and refinement: SHELX-97 (G. M. Sheldrick, SHELXS-97, Program for the Solution of Crystal Structures, Universität Göttingen, 1997). CCDC-665724 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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