Expeditious microwave-assisted thionation with the system PSCl 3/H2O/Et3N under solvent-free condition (Journal of Organic Chemistry (2008) 73, (2890) DOI: 10.1021/jo7022069);Expeditious microwave-assisted thionation with the system PSCl 3/H2O/Et3N under solvent-free condition

Journal of Organic Chemistry

Volumn 73, Issue 7, 2008, Pages 2890-2893

  Pathak, Uma ^a   Pandey, Lokesh Kumar ^a   Tank, Rekha ^a  

^a DEFENCE RESEARCH AND DEVELOPMENT ESTABLISHMENT   (India)

Author keywords

[No Author keywords available]

Indexed keywords

MICROWAVE IRRADIATION; SOLVENTS; SYNTHESIS (CHEMICAL);

CARBONYL COMPOUNDS; SOLVENT FREE CONDITION;

KETONES;

ACRIDONE DERIVATIVE; CARBONYL DERIVATIVE; LACTAM DERIVATIVE; SOLVENT; THIOAMIDE; THIOKETONE; THIOL DERIVATIVE; THIOXANTHENE DERIVATIVE;

ARTICLE; BIOTRANSFORMATION; CHEMICAL REACTION; COVALENT BOND; MICROWAVE IRRADIATION; MOLECULAR MECHANICS; ORGANIC CHEMISTRY; REACTION ANALYSIS; THIONATION;

EID: 41649117563     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo902133a     Document Type: Erratum

References (39)

1. (a) Bernardi, F., Csizmadia, I. G., Mangini, A., Eds. Organic Sulfur Chemistry; Elsevier: New York, 1985.
2. (b) Damani, L. A. Sulfur-containing Drugs and Related Organic Compounds-Chemistry, Biochemistry and Toxicology; Ellis Harwood: Chichester, 1989.
3. (c) Block, E. Reactions of organosulfur compounds; Academic Press: New York, 1978.
4. (d) Cremlyn, R. J. An Introduction to Organosulfur Chemistry; John Wiley & Sons: New York, 1996.
5. (e) Shaumann, E. Synthesis of Thioamides and Thiolactams. In Comprehensive Organic Synthesis; Trost, B. M., Fleming, I., Winterfeldt, E., Eds.; Pergamon Press: New York, 1991; Vol. 6, pp 419-434.
6. (f) Duus, F. Thiocarbonyl Compounds. In Comprehensive Organic Chemistry; Jones, D. N., Ed.;
7. (g) Brillion, D. Sulfur Rep. 1992, 1, 297.
8. (h) Polshettiwar, V.; Kaushik, M. P. J. Sulfur Chem. 2006, 27, 353-386.
9. (a) Jesberger, M.; Davis, T. P.; Barner, L. Synthesis 2003, 1929-1958.
10. (b) Cava, M. P.; Levinson, M. I. Tetrahedron 1985, 41, 5061-5087.
11. (c) Scheibye, S.; Pedersen, B. S.; Lawesson, S. O. Bull. Soc. Chim. Belg. 1978, 87, 229-238.
12. (d) Kaleta, Z.; Makowski, B.T.; Soos, T.; Dembinski, R. Org. Lett. 2006, 8, 1625-1628.
13. (a) Hurd, R. N.; DeLaMater, G. Chem. Rev. 1961, 61, 45.
14. (b) Wakabayashi, T.; Kato, Y.; Watanabe, K. Jpn. Kokai Tokkyo Koho 1978, 78, 56, 662; Chem. Abstr. 1979, 90, 22818h.
15. (c) Brillon, D. Sulfur Rep. 1992, 12, 297-338.
16. (d) Curphey, T. J. J. Org. Chem. 2002, 67, 6461-6473.
17. (a) Asquith, R. S.; Hammick, D. Ll.; Williams, P. L. J. Chem. Soc. 1948, 1181
18. (b) Fournier, C.; Paquer, D.; Vazeux, M. Bull. Soc. Chim. Fr. 1975, 2753.
19. (c) Sen, D. C. J. Indian Chem. Soc. 1935, 12, 647;
20. 1937, 14, 214.
21. Zong, Z.-M.; Peng, Y.-L.; Liu, Z.-G.; Zhou, S.-L.; Wu, L.; Wang, X.-H.; Wei, X.-Y.; Lee, C. W. Korean J. Chem. Eng. 2003, 20(2), 235-238.
22. (a) Oae, S.; Nakanishi, A.; Tsujimoto, N. Chem. Ind. 1972, 575.
23. (b) Pedersen, B. S.; Lawesson, S. O.; Bull. Soc. Chim. Belg. 1977, 86, 693.
24. Ishii, Y.; Hirabayashi, T.; Imaeda, H.; Ito, Jpn, K. Patent 40441, 1974; Chem. Abstr. 1975, 82, 156074f.
25. Bodine, J. J.; Kaloustian, M. K. Synth. Commun. 1982, 12, 787.
26. Smith, D. C.; Lee, S. W.; Fuchs, P. L. J. Org. Chem. 1994, 59, 348-354.
27. (a) Pedersen, B. S.; Scheibye, S.; Nilsson, N. H.; Lawesson, S. O. Bull. Soc. Chim. Belg. 1978, 87, 223-228.
28. (b) Yang C. O-; Rotstein, D. M.; Labadie, S.S.; Walker K. A. M. Synlett, 1995, 655.
29. Charette, A. B.; Grenon, M. J. Org. Chem. 2003, 68, 5792-5794.
30. (a) Dean, F. M.; Goodchild, J.; Hill, A. W. J. Chem. Soc. (c), 1969, 2192-2195.
31. (b) Dean, F. M.; Goodchild, J.; Hill, A. W.; Moore, S.; Zahman, A. J. Chem. Soc., Perkin Trans. 1 1975, 1335.
32. Degl'Innocenti, A.; Capperucci A.; Castagnoli G.; Malesci. I. Synlett 1965 (2005).
33. (a) Perrenaard, J.; Pedersen, B. S.; Lawesson, S.-O. Acta Chem. Scand. B31.460 (1977)
34. (b) Pipko, S. E.; Simurova, N. V.; Shvadchak, V. V.; Bezgubenko, L. V.; Luk'yaneko, S. N. Russ. J. Gen. Chem. 2006, 76, 1019-1021.
35. (a) Barton, D. H. R. U. S. Patent 4011316, 1977; Chem Abstr. 1977, 87, 53490n.
36. (b) Machiguchi, T.; Hoshino, M.; Kitahara, Y. Jpn. Kokai Tokkyo Koho 77,23,066, 1977; Chem. Abstr. 1977, 82, 102153r.
37. (a) Loupy, A., Ed. Microwave in Organic Synthesis; Wiley-VCH: Weinheim, 2002.
38. (b) Varma, R. S.; Kumar, D. Org. Lett. 1999, 1, 697-700.
39. 3 and water (0.005 mol) was taken in a test tube. To this triethyl amine was added dropwise at 0-5°C with constant stirring till the contents were basic, this is followed by slow addition of 0.005 mol 1-vinyl-2-pyrrolidinone. Reaction mixture is then microwaved at 180 W for 3-4 min. Work up was carried by following the reaction workup procedure, method A.