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3 Their attempted conversion of acid 9 to the exo enone intermediate by treatment with formaldehyde and piperidine led to a complex mixture of products. In our hands the sequence was successful with very careful handling but was not easily scalable.
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3 Their attempted conversion of acid 9 to the exo enone intermediate by treatment with formaldehyde and piperidine led to a "complex mixture of products." In our hands the sequence was successful with very careful handling but was not easily scalable.
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