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Approximately 0.2 g of reaction mass was dissolved in 50 mL of dichloromethane and acetic acid (4/1 solution, ratio). Enough amount of TBAI was added and dissolved. Afterwards, the conversion of the addition reaction was checked by titration of the above sample with 0.1 M-Perchlo-ric acid.
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Approximately 0.2 g of reaction mass was dissolved in 50 mL of dichloromethane and acetic acid (4/1 solution, volume ratio). Enough amount of TBAI was added and dissolved. Afterwards, the conversion of the addition reaction was checked by titration of the above sample with 0.1 M-Perchlo-ric acid.
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