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Volumn 11, Issue 4, 2008, Pages 438-441

μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization

Author keywords

Copper(II) complexes; Crystal structure; Magnetic properties; Oxalato bridged; Polynuclear complexes

Indexed keywords


EID: 41049088339     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2008.01.019     Document Type: Article
Times cited : (14)

References (44)
  • 32
    • 41049099740 scopus 로고    scopus 로고
    • note
    • 18: C, 30.31; H, 5.48; N, 10.56%. Found: C, 30.36; H, 5.56; N, 10.83%. Caution: Salts of perchlorate and their metal complexes are potentially explosive and should be handled with great care and in small quantities.
  • 33
    • 41049103637 scopus 로고    scopus 로고
    • note
    • -3; Bruker-AXS SMART APEX CCD diffractometer, λ = 0.71073 Å, programs used: SADABS, SHELXS-86, SHELXL-93 incorporated in the SHELXTL/PC V 5.03 program package.
  • 36
    • 41049104397 scopus 로고    scopus 로고
    • note
    • Physical measurements: Infrared spectra were recorded on JASCO FT/IR-480 plus spectrometer as KBr pellets. Electronic spectra were recorded using Agilent 8453 HP diode UV-vis spectrophotometer. Elemental analysis was performed at the Atlantic Microlaboratory (Norcross, Georgia USA). Magnetic susceptibility measurements (2-300 K) and magnetization measurements in the field range of 0.4-1 T were performed with a Quantum Design MPMS-XL SQUID magnetometer at the Magnetochemistry Service of the University of Barcelona. All measurements were performed on polycrystalline samples. Data were corrected for the magnetization of the sample holder and for diamagnetic contributions, which were estimated from Pascal's constants.
  • 37
    • 0000684712 scopus 로고
    • Wilkinson G., Gillard R.D., and McCleverty J.A. (Eds), Pergamon, Press, Oxford, England
    • Hathaway B.J. In: Wilkinson G., Gillard R.D., and McCleverty J.A. (Eds). Comprehensive Coordination Chemistry Vol. 5 (1987), Pergamon, Press, Oxford, England 533
    • (1987) Comprehensive Coordination Chemistry , vol.5 , pp. 533
    • Hathaway, B.J.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.