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Volumn 37, Issue 2, 2008, Pages 166-167

Synthesis of a hetero-bimetallic complex with an inorganic cyclic framework using a bis(iminophosphorane)iron complex as a chelating ligand

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Indexed keywords

EID: 40449091053 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2008.166 Document Type: Article

Times cited : (3)

References (14)

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- Analytical data for 4: IR (vCO, in THF, 1919 cm-1. 1HNMR (δ, in C6D6) 1.37 (m, 2H, cod, 1.63 (s, 15H, C5(CH3)5, 1.66 (m, 2H, cod, 2.11 (br, 2H, cod, 2.69 (br, 2H, cod, 3.27 (t, JHP, 5.1 Hz, 6 H, OCH3, 3.53 (br, 2H, cod, 3.64 (t, JHP, 5.9 Hz, 6H, OCH3, 4.20 (br, 2H, cod, 7.02-7.98 (m, 10H, C 6H5, 13C{1H}NMR (δ, in C 6D6, 9.6 (s, C5(CH3)5, 29.8 (s, cod, 30.8 (s, cod, 50.0 (s, OCH3, 53.4 (t, J CP, 3.8Hz, OCH3, 78.0 (d, JCRh, 12.3Hz, cod, 81.1 (d, JCRh, 13.7Hz, cod, 95.8 (s, C 5(CH3)5, 121.1 (s, C6H 5, 127.7 (t, JCP, 4.7 Hz, C6H 5, 128.3 s
- 2Rh: C, 52.65; H, 6.19; N, 3.51%. Found: C, 52.42; H, 6.38; N, 3.42%.

11
- 40449142866
- Crystallographic data for 4 have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-664797. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 IEZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).
- Crystallographic data for 4 have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-664797. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 IEZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk).

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